1-甲硫基-N-(1-苯基亚乙基氨基)硫代甲酰胺合成路线 （共 9 条）
反应条件
hydrogenchloride in ethanol 24 h; Heating;
参考文献
Lin, Ai Jeng; Klayman, Daniel L.
Journal of Heterocyclic Chemistry, 1985 , vol. 22, p. 1 - 4
反应条件
potassium hydroxide; hydrazine 1.) ethanol, 0 deg C, 1 h, 2.) ethanol, from 0 deg C to RT, 3 h; Multistep reaction;
参考文献
Shimada, Kazuaki; Otaki, Akihiro; Yanakawa, Masaki; Mabuchi, Shosuke; Yamakado, Naoya; Shimoguchi, Takeshi; Inoue, Kazuya; Kagawa, Takashi; Shoji, Kazutoshi; Takikawa, Yuji
Bulletin of the Chemical Society of Japan, 1996 , vol. 69, # 4 p. 1043 - 1054
反应条件
in benzene mixt. of In(III) isopropoxide and thio-Schiff base (molar ratio 1:2) in dry benzene refluxed under fractionating column for 7 h in oil bath at 110°C; benzene removed under reduced pressure, recrystd. from hexane and benzene (1:1), elem. anal.;
参考文献
Baskaran, S.; Kapoor, Ramesh N
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1983 , vol. 13, p. 305 - 320
参考文献
Kulandaivelu, Umasankar; Shireesha, Boyapati; Mahesh, Chidara; Vidyasagar, Jannu Vincent; Rao, Tadikonda Rama; Jayaveera; Saiko, Philipp; Graser, Geraldine; Szekeres, Thomas; Jayaprakash, Venkatesan
Medicinal Chemistry Research, 2013 , vol. 22, # 6 p. 2802 - 2808
反应条件
in ethanol
addn. of Cu(NO3)2 to 2 equiv. of ligand, heating for 10 min; cooling in ice (crystn.), collection, washing (ice-cold alcohol), drying(vac., over silica gel); elem. anal.;
参考文献
Das; Livingstone
Inorganica Chimica Acta, 1976 , vol. 19, p. 5
反应条件
in ethanol
addn. of Zn(NO3)2 to 2 equiv. of ligand, heating for 10 min; cooling in ice or refrigerating overnight (crystn.), collection, washing(ice-cold alcohol), drying (vac., over silica gel); elem. anal.;
参考文献
Das; Livingstone
Inorganica Chimica Acta, 1976 , vol. 19, p. 5
反应条件
in ethanol; water
slow addn. of aq. K2PdCl4 to stirred soln. of 2 equiv. of ligand in hot alcohol, heating (steam bath, 10 min; pptn.); hot filtration, washing (water, alcohol), drying (vac., over silica gel); elem. anal.;
参考文献
Das; Livingstone
Inorganica Chimica Acta, 1976 , vol. 19, p. 5
反应条件
in ethanol; water
slow addn. of aq. K2PtCl4 to stirred soln. of 2 equiv. of ligand in hot alcohol, heating (steam bath, 10 min; pptn.); hot filtration, washing (water, alcohol), drying (vac., over silica gel); elem. anal.;
参考文献
Das; Livingstone
Inorganica Chimica Acta, 1976 , vol. 19, p. 5
反应条件
in ethanol
addn. of Ni(NO3)2 to 2 equiv. of ligand, heating for 10 min; cooling in ice (crystn.), collection, washing (ice-cold alcohol), drying(vac., over silica gel); elem. anal.;
参考文献
Das; Livingstone
Inorganica Chimica Acta, 1976 , vol. 19, p. 5
