1,3,3-三甲基-1,2-二氢茚合成路线 （共 23 条）
反应条件
BF3*AcOH in dichloromethane T=0°C; 0.25 h;
参考文献
Fleming, Ian; Patel, Shailesh K.; Urch, Christopher J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 115 - 124
反应条件
copper T=404 - 454°C; P=308913 Torr;
参考文献
Schaap; Pines
Journal of the American Chemical Society, 1957 , vol. 79, p. 4967,4968
反应条件
methanol; nickel Hydrogenation;
参考文献
Gelin,R.; Chantegrel,B.
Bulletin de la Societe Chimique de France, 1971 , p. 2527 - 2544
反应条件
1: diethyl ether 3: Raney nickel; methanol / Hydrogenation View Scheme
参考文献
Gelin,R.; Chantegrel,B.
Bulletin de la Societe Chimique de France, 1971 , p. 2527 - 2544
反应条件
phosphorus pentoxide Heating;
参考文献
Condon, Francis E.; West, David L.
Journal of Organic Chemistry, 1980 , vol. 45, p. 2006 - 2009
反应条件
1: AlCl3 2: diethyl ether 3: H2 / Pd-C / ethyl acetate View Scheme
参考文献
Gelin,R.; Chantegrel,B.
Bulletin de la Societe Chimique de France, 1971 , p. 2527 - 2544
反应条件
1: AlCl3 2: diethyl ether 3: H2 / Pd-C / ethyl acetate View Scheme
参考文献
Gelin,R.; Chantegrel,B.
Bulletin de la Societe Chimique de France, 1971 , p. 2527 - 2544
反应条件
trifluorormethanesulfonic acid; carbon monoxide; 2-methyl-but-1(2)-ene in tetrachloromethane P=79800.1 Torr; 3 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Booth, Brian L.; El-Fekky, Teymour A.; Noori, Ghazi F. M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 181 - 186
反应条件
hydrogen; Ra-Ni in methanol 3 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Miethchen, Ralf; Steege, Sigrid; Kroeger, Carl-Friedrich
Journal fuer Praktische Chemie (Leipzig), 1983 , vol. 325, # 5 p. 823 - 834
反应条件
1: 95 percent / tetrahydrofuran / 2 h / Heating 2: 82 percent / BF3*2AcOH / CH2Cl2 / 0.25 h / 0 °C View Scheme
参考文献
Fleming, Ian; Patel, Shailesh K.; Urch, Christopher J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 115 - 124
