2-吡啶-3-基-1,3-苯并噻唑合成路线 （共 17 条）
反应条件
Cu(II) containing nanosilica triazine dendrimer in neat (no solvent)
T=20°C; 1.5 h; Catalytic behavior;
参考文献
Nasr-Esfahani, Mahboobeh; Mohammadpoor-Baltork, Iraj; Khosropour, Ahmad Reza; Moghadam, Majid; Mirkhani, Valiollah; Tangestaninejad, Shahram
Journal of Molecular Catalysis A: Chemical, 2013 , vol. 379, p. 243 - 254
反应条件
1-propanephosphonic acid cyclic anhydride; N-ethyl-N,N-diisopropylamine in ethyl acetate
T=100°C; 0.166667 h; Microwave irradiationSealed tube;
参考文献
Wen, Xiaoan; Bakali, Jamal El; Deprez-Poulain, Rebecca; Deprez, Benoit
Tetrahedron Letters, 2012 , vol. 53, # 19 p. 2440 - 2443
反应条件
1,4-diaza-bicyclo[2.2.2]octane; 1,10-phenanthroline; copper (II) acetate monohydrate; sulfur in dimethyl sulfoxide
T=100°C;
参考文献
Wang, Rui; Ding, Yong-Liang; Liu, Hong; Peng, Shu; Ren, Jie; Li, Lei
Tetrahedron Letters, 2014 , vol. 55, # 4 p. 945 - 949
反应条件
copper(I) thiophene-2-carboxylate; trifuran-2-yl-phosphane; zinc diacetate; tris-(dibenzylideneacetone)dipalladium(0) in tetrahydrofuran
T=50°C; 18 h;
参考文献
Liebeskind, Lanny S; Srogl, Jiri
Organic letters, 2002 , vol. 4, # 6 p. 979 - 981
反应条件
sodium hydroxide in (2S)-N-methyl-1-phenylpropan-2-amine hydrate; chloroform
参考文献
E. R. Squibb and Sons, Inc.
Patent: US3985885 A1, 1976 ;
反应条件
[2,2']bipyridinyl; [Ni(O2CCH3)2]*4H2O; Mg(O-t-Bu)2 in N,N-dimethyl-formamide
T=100°C; 36 h; Inert atmosphere;
参考文献
Yamamoto, Takuya; Muto, Kei; Komiyama, Masato; Canivet, Jerome; Yamaguchi, Junichiro; Itami, Kenichiro
Chemistry - A European Journal, 2011 , vol. 17, # 36 p. 10113 - 10122
反应条件
PdCl(C3H5)(1,4-bis(diphenylphosphino)butane); caesium carbonate in N,N-dimethyl-formamide
T=150°C; 20 h; Inert atmosphere;
参考文献
Derridj, Fazia; Roger, Julien; Geneste, Florence; Djebbar, Safia; Doucet, Henri
Journal of Organometallic Chemistry, 2009 , vol. 694, # 3 p. 455 - 465
反应条件
1: 2-amino-benzenethiol With trimethylaluminum chloride in toluene
T=0 - 20°C;
2: hydroxymethyl JandaJelTM resin-bound 3-pyridyl ester in toluene
24 h; Heating; Further stages.;
参考文献
Matsushita, Hana; Lee, Sang-Hyeup; Joung, Meyoungju; Clapham, Bruce; Janda, Kim D.
Tetrahedron Letters, 2004 , vol. 45, # 2 p. 313 - 316
反应条件
{PdCl2[(t-Bu)2PCl]2}; Cu[9,9-dimethyl-4,5-bis(diphenylphosphine)xanthene]I; caesium carbonate in toluene
T=100°C; Inert atmosphere;
参考文献
Huang, Jinkun; Chan, Johann; Chen, Ying; Borths, Christopher J.; Baucom, Kyle D.; Larsen, Robert D.; Faul, Margaret M.
Journal of the American Chemical Society, 2010 , vol. 132, # 11 p. 3674 - 3675
反应条件
sulfur in neat (no solvent)
T=120°C; 20 h; Inert atmosphere;
参考文献
Nguyen, Thanh Binh; Ermolenko, Ludmila; Dean, William A.; Al-Mourabit, Ali
Organic Letters, 2012 , vol. 14, # 23 p. 5948 - 5951
