(4-氰基苄基)(三苯基)溴化膦合成路线 (共 10 条)
反应条件
in toluene 6 h; Heating;
参考文献
Mylona, Anastasia; Nikokavouras, John; Takakis, Ioannis M.
Journal of Chemical Research, Miniprint, 1986 , # 12 p. 3514 - 3530
参考文献
Corsane, M.; Defay, N.; Martin, R. H.
Bulletin des Societes Chimiques Belges, 1985 , vol. 94, # 3 p. 215 - 232
反应条件
potassium hydroxide; 18-crown-6 ether in dichloromethane T=-70°C;
参考文献
Bellucci, Giuseppe; Chiappe, Cinzia; Lo Moro, Giacomo
Tetrahedron Letters, 1996 , vol. 37, # 24 p. 4225 - 4228
反应条件
iodine; lithium hexamethyldisilazane 1.) THF, 2.) CCl4, reflux, irrad., 24 h; Multistep reaction;
参考文献
He, Gong-Xin; Mei, Houng-Yau; Bruice, Thomas C.
Journal of the American Chemical Society, 1991 , vol. 113, # 15 p. 5644 - 5650
反应条件
sodium ethanolate in ethanol 3.5 h;
参考文献
Das; Zalkow; Forrester; Molock; Boykin
Journal of Pharmaceutical Sciences, 1982 , vol. 71, # 4 p. 465 - 466
反应条件
sodium hydroxide; nitrogen(II) oxide in dichloromethane T=20°C; 5 h;
参考文献
Tetrahedron Letters, , vol. 46, # 7 p. 1095 - 1097
反应条件
sodium hydride in diethyl ether
1.) two days, ultrasonic bath, 2.) 10-15 min.; Yield given;
参考文献
Rafizadeh, Karim; Yates, Keith
Journal of Organic Chemistry, 1984 , vol. 49, # 9 p. 1500 - 1506
反应条件
in acetonitrile
Irradiationother group V-onium salts; Product distributionMechanism;
参考文献
Breslin, David T.; Saeva, Franklin D.
Journal of Organic Chemistry, 1988 , vol. 53, # 4 p. 713 - 715
反应条件
sodium hydroxide; nitrogen(II) oxide in dichloromethane
T=20°C; 5 h;
参考文献
Liu, Zhongquan; Zhou, Bo; Liu, Zhongli; Wu, Longmin
Tetrahedron Letters, 2005 , vol. 46, # 7 p. 1095 - 1097
反应条件
in acetonitrile
Irradiationother group V-onium salts; Product distributionMechanism;
参考文献
Breslin, David T.; Saeva, Franklin D.
Journal of Organic Chemistry, 1988 , vol. 53, # 4 p. 713 - 715