7-氨基-4-甲基香豆素合成路线 （共 67 条）
反应条件
zirconium orthophosphate T=110°C; Pechmann condensation; 0.166667 h; Microwave irradiation; chemoselective reaction;
参考文献
Sinhamahapatra, Apurba; Sutradhar, Narottam; Pahari, Sandip; Bajaj, Hari C.; Panda, Asit Baran
Applied Catalysis A: General, 2011 , vol. 394, # 1-2 p. 93 - 100
反应条件
sulfuric acid in acetic acid T=120°C; 4 h; Reflux;
参考文献
UNIVERSITY OF DELHI; VALLABHBHAI PATEL CHEST INSTIUTE; PARMAR, Virinder Singh; PRASAD, Ashok Kumar; RAJ, Hanumantharao Guru; BOSE, Mridula; SHARMA, Sunil Kumar; TONDON, Rashmi; BAGHEL, Anil; KATHURIA, Abha; GUPTA, Garima; AGGARWAL, Neha
Patent: WO2012/137224 A1, 2012 ;
Location in patent: Page/Page column 13-14 ;
反应条件
potassium hydroxide T=80 - 90°C; 0.333333 h;
参考文献
Ji, Weidong; Li, Najun; Chen, Dongyun; Qi, Xiuxiu; Sha, Wenwei; Jiao, Yang; Xu, Qingfeng; Lu, Jianmei
Journal of Materials Chemistry B, 2013 , vol. 1, # 43 p. 5942 - 5949
反应条件
α-chymotrypsine in carbon dioxide; water T=45°C; P=75007.5 Torr; 2 h;
参考文献
Knuettel, Torsten; Meyer, Hartmut; Scheper, Thomas
Analytical Chemistry, 2005 , vol. 77, # 19 p. 6184 - 6189
反应条件
1: 94 percent / KHCO3 / ethyl acetate; H2O / 4 h 2: 87.5 percent / conc. H2SO4 / 2 h 3: 83 percent / 45percent aq. KOH / 0.33 h / 80 - 90 °C View Scheme
参考文献
Karami, Bahador; Khodabakhshi, Saeed; Eskandari, Khalil
Chemical Papers, 2013 , vol. 67, # 11 p. 1474 - 1478
反应条件
bismuth(III) chloride T=75°C; Pechmann condensation; 1 h;
参考文献
De, Surya K.; Gibbs, Richard A.
Synthesis, 2005 , # 8 art. no. M08304SS, p. 1231 - 1233
反应条件
silver hexafluoroantimonate; PPh3 gold(I) chloro complex in 1,4-dioxane; 1,2-dichloro-ethane T=20°C; Sealed tube; Overall yield = 95 percent; Overall yield = 100 mg;
参考文献
Vadola, Paul A.; Sames, Dalibor
Journal of Organic Chemistry, 2012 , vol. 77, # 18 p. 7804 - 7814,11
反应条件
1: 87.5 percent / conc. H2SO4 / 2 h 2: 83 percent / 45percent aq. KOH / 0.33 h / 80 - 90 °C View Scheme
参考文献
Habashneh, Almeqdad Y.; El-Abadelah, Mustafa M.; Abadleh, Mohammed M.; Voelter, Wolfgang
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2012 , vol. 67, # 7 p. 725 - 730
反应条件
recombinant human caspase-1 in dimethyl sulfoxide T=20°C; pH=7.4; Enzyme kinetics;
参考文献
Le, Giang Thanh; Abbenante, Giovanni; Madala, Praveen K.; Hoang, Huy N.; Fairlie, David P.
Journal of the American Chemical Society, 2006 , vol. 128, # 38 p. 12396 - 12397
反应条件
potassium hydroxide in dimethyl sulfoxide T=140°C; 2 h;
参考文献
Yu, Jianzhong; Wang, Yongtao; Zhang, Peizhi; Wu, Jun
Synlett, 2013 , vol. 24, # 11 art. no. ST-2013-W0237-L, p. 1448 - 1454
