2,6-二叔-丁基-4-亚甲基环己-2,5-二烯-1-酮合成路线 (共 32 条)
反应条件
triethylamine in pentane T=6°C; few minutes;
参考文献
Omura, Kanji
Journal of Organic Chemistry, 1992 , vol. 57, # 1 p. 306 - 312
反应条件
DPPH-H; Butylated hydroxyanisole in benzene T=20°C; Rate constantMechanism;
参考文献
Lewis, Mark A.; Yoerg, Darla Graff; Bolton, Judy L.; Thompson, John A.
Chemical Research in Toxicology, 1996 , vol. 9, # 8 p. 1368 - 1374
反应条件
(i) HCl, CH2Cl2, (ii) K2CO3; Multistep reaction;
参考文献
Goulart, Marilia O. F.; Utley, James H. P.
Journal of Organic Chemistry, 1988 , vol. 53, # 11 p. 2520 - 2525
反应条件
1: 47 percent / 1 M aq. NaOH, sodium borohydride / methanol / 27 h / Ambient temperature 2: trimethylsilyl chloride / CH2Cl2 / 3 h View Scheme
参考文献
Pospisek,J. et al.
Collection of Czechoslovak Chemical Communications, 1975 , vol. 40, p. 142 - 148
反应条件
cobalt(III) acetate in acetic acid T=50°C; 15 h;
参考文献
Hirano, Masao; Ishii, Tadamichi; Morimoto, Takashi
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 4 p. 1434 - 1436
反应条件
1: 49 percent / NBS; AIBN / CCl4 / Irradiation View Scheme
参考文献
Rabin, Oded; Vigalok, Arkadi; Milstein, David
Chemistry - A European Journal, 2000 , vol. 6, # 3 p. 454 - 462
反应条件
methanol; trifluorormethanesulfonic acid T=30°C; 0.35 h;
参考文献
Omura, Kanji
Journal of Organic Chemistry, 2008 , vol. 73, # 3 p. 858 - 867
反应条件
potassium acetate in water T=100°C; 0.5 h;
参考文献
Barton, Benita; Logie, Catherine G.; Schoonees, Barbara M.; Zeelie, Bernard
Organic Process Research and Development, 2005 , vol. 9, # 1 p. 62 - 69
反应条件
in acetic acid T=50°C; 15 h;
参考文献
Hirano, Masao; Ishii, Tadamichi; Morimoto, Takashi
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 4 p. 1434 - 1436
参考文献
Tajima; Yamamoto; Mizutani
Chemical and Pharmaceutical Bulletin, 1981 , vol. 29, # 12 p. 3738 - 3741