1-甲氧基-4-(1-苯基乙基)-苯合成路线 (共 39 条)
反应条件
oxygen T=120 - 140°C;
参考文献
Grushin, A. I.; Grigor'ev, V. V.; Prokof'ev, K. V.; Kozlova, N. M.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 10 p. 1991 - 1993
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 10 p. 2176 - 2178
反应条件
[Fe(III)(TPP)]SbF6 in 1,2-dichloro-ethane
T=80°C; Friedel-Crafts Alkylation; 5 h; Sealed tubeInert atmosphere; regioselective reaction;
参考文献
Teranishi, Satoru; Kurahashi, Takuya; Matsubara, Seijiro
Synlett, 2013 , vol. 24, # 16 art. no. ST-2013-U0620-L, p. 2148 - 2152
反应条件
H-β-zeolite in cyclohexane
T=80°C; 6 h;
参考文献
Mohan, Darapaneni Chandra; Patil, Rajendra D.; Adimurthy, Subbarayappa
European Journal of Organic Chemistry, 2012 , # 18 p. 3520 - 3525
反应条件
1,3-bis-(diphenylphosphino)propane; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in various solvent(s)
T=140°C; 16 h;
参考文献
Fessard, Thomas C.; Andrews, Stephen P.; Motoyoshi, Hajime; Carreira, Erick M.
Angewandte Chemie - International Edition, 2007 , vol. 46, # 48 p. 9331 - 9334
反应条件
dichloro bis(acetonitrile) palladium(II); 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in tetrahydrofuran
T=20°C; Kumada-Corriu reaction; 14 h; Inert atmosphere;
参考文献
Lopez-Perez, Ana; Adrio, Javier; Carretero, Juan C.
Organic Letters, 2009 , vol. 11, # 23 p. 5514 - 5517
反应条件
tetrafluoroboric acid; dicobalt octacarbonyl; 4-laurylbenzenesulfonic acid sodium salt in benzene
T=55°C; 4 h;
参考文献
Alper, Howard; Heveling, Josef
Journal of the Chemical Society, Chemical Communications, 1983 , # 7 p. 365 - 366
反应条件
[Fe(III)(TPP)]SbF6 in 1,2-dichloro-ethane
T=80°C; Friedel-Crafts Alkylation; 5 h; Sealed tubeInert atmosphere;
参考文献
Teranishi, Satoru; Kurahashi, Takuya; Matsubara, Seijiro
Synlett, 2013 , vol. 24, # 16 art. no. ST-2013-U0620-L, p. 2148 - 2152
反应条件
1: 1-bromo-4-methoxy-benzene With 3-chloroprop-1-ene; trifluoroacetic acid; cobalt(II) dibromide; zinc in acetonitrile
T=20°C;
2: 1-chloro-1-phenylethane in acetonitrile
T=20°C; Barbier type reductive cross-coupling;
参考文献
Amatore, Muriel; Gosmini, Corinne
Chemical Communications, 2008 , # 40 p. 5019 - 5021
反应条件
trifluorormethanesulfonic acid
T=100°C; 0.5 h; Neat (no solvent);
参考文献
Mendoza, Oscar; Rossey, Guy; Ghosez, Leon
Tetrahedron Letters, 2011 , vol. 52, # 17 p. 2235 - 2239
反应条件
in n-heptane; 1,2-dichloro-ethane
T=50°C; 16 h;
参考文献
Mahoney, Stuart J.; Lou, Tiantong; Bondarenko, Ganna; Fillion, Eric
Organic Letters, 2012 , vol. 14, # 13 p. 3474 - 3477