(4-乙酰基苯基)-磷酸二乙酯合成路线 (共 12 条)
反应条件
triethylamine; tetrakis(triphenylphosphine) palladium(0) in toluene T=90°C; 8 h;
参考文献
Wang, Ping; Lu, Jie; Zhang, Zhan-Hui
Journal of Chemical Research, 2013 , vol. 37, # 6 p. 359 - 361
反应条件
copper(I) oxide; 1,10-phenanthroline; N-ethyl-N,N-diisopropylamine in acetonitrile T=20°C; 24 h;
参考文献
Zhuang, Rongqiang; Xu, Jian; Cai, Zhenshi; Tang, Guo; Fang, Meijuan; Zhao, Yufen
Organic Letters, 2011 , vol. 13, # 8 p. 2110 - 2113
反应条件
palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether in tetrahydrofuran T=25°C; Hirao reaction; 16 h; Inert atmosphereDarkness;
参考文献
Kohler, Mark C.; Sokol, Joseph G.; Stockland Jr., Robert A.
Tetrahedron Letters, 2009 , vol. 50, # 4 p. 457 - 459
反应条件
palladium diacetate; caesium carbonate; potassium iodide in acetonitrile T=20 - 80°C; Inert atmosphere;
参考文献
Berrino, Roberta; Cacchi, Sandro; Fabrizi, Giancarlo; Goggiamani, Antonella; Stabile, Paolo
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 20 p. 4518 - 4520
反应条件
nickel dichloride in neat (no solvent) T=160°C; Arbuzov Reaction; Microwave irradiation;
参考文献
Keglevich, Gyoergy; Gruen, Alajos; Boelcskei, Adrienn; Drahos, Laszlo; Kraszni, Marta; Balogh, Gyoergy T.
Heteroatom Chemistry, 2012 , vol. 23, # 6 p. 574 - 582
反应条件
NiII chloride hexahydrate; potassium bromide T=185 - 190°C; Arbuzov reaction; 20 h; Inert atmosphere;
参考文献
Yang, Guoqiang; Shen, Chaoren; Zhang, Liang; Zhang, Wanbin
Tetrahedron Letters, 2011 , vol. 52, # 39 p. 5032 - 5035
反应条件
2,9-dimethyl-1,10-phenanthroline; palladium (II) trifluoroacetate; p-benozquinone in methanol T=120°C; 0.333333 h; Microwave irradiation;
参考文献
Andaloussi, Mounir; Lindh, Jonas; Saevmarker, Jonas; Sjoeberg, Per J. R.; Larhed, Mats
Chemistry - A European Journal, 2009 , vol. 15, # 47 p. 13069 - 13074
反应条件
1: 4-hydroxy-acetophenone With potassium carbonate; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate in acetonitrile T=100°C; 3 h; Inert atmosphere; 2: phosphonic acid diethyl ester With [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in acetonitrile T=120°C; 10 h; Inert atmosphere;
参考文献
Zhao, Yu-Long; Wu, Guo-Jie; Han, Fu-She
Chemical Communications, 2012 , vol. 48, # 47 p. 5868 - 5870
反应条件
tetrakis(triphenylphosphine) palladium(0); triethylamine T=130°C; 20 h; Green chemistry;
参考文献
Wang, Ping; Lu, Jie; Zhang, Zhan-Hui
Journal of Chemical Research, 2013 , vol. 37, # 6 p. 359 - 361
反应条件
nickel dichloride T=165 - 175°C; 0.0833333 h;
参考文献
Sentemov, V. V.; Krasil'nikova, E. A.; Berdnik, I. V.
J. Gen. Chem. USSR (Engl. Transl.), 1989 , vol. 59, # 12.1 p. 2406 - 2407