1,3-二(1,2-二溴乙基)苯合成路线 （共 7 条）
反应条件
bromine in tetrachloromethane 0 ceg C to r.t.;
参考文献
Ghose
Journal fur Praktische Chemie, 1982 , vol. 324, # 6 p. 1052 - 1054
反应条件
1: 95 percent / LiOEt / ethanol / 2 h / Ambient temperature 2: 82 percent / Br2 / CCl4 / 0 ceg C to r.t. View Scheme
参考文献
Mitchell,R.H. et al.
Canadian Journal of Chemistry, 1977 , vol. 55, p. 210 - 219
反应条件
1: 198.0 g / dimethylformamide / 2 h / 180 °C 2: 95 percent / LiOEt / ethanol / 2 h / Ambient temperature 3: 82 percent / Br2 / CCl4 / 0 ceg C to r.t. View Scheme
参考文献
Mitchell,R.H. et al.
Canadian Journal of Chemistry, 1977 , vol. 55, p. 210 - 219
反应条件
hydrogen bromide; acetic acid
参考文献
Ruggli; Knecht
Helvetica Chimica Acta, 1944 , vol. 27, p. 1108,1115
反应条件
1: chloroform; PBr3 2: bei der Destillation 3: chloroform; bromine / 0 °C View Scheme
参考文献
Deluchat
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1931 , vol. 192, p. 1387
Annales de Chimie (Cachan, France), 1934 , vol. <11> 1, p. 181,224
反应条件
1: bei der Destillation 2: chloroform; bromine / 0 °C View Scheme
参考文献
Deluchat
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1931 , vol. 192, p. 1387
Annales de Chimie (Cachan, France), 1934 , vol. <11> 1, p. 181,224
反应条件
potassium tert-butylate in 1,4-dioxane; tert-butyl alcohol 1 h; Ambient temperature;
参考文献
Journal fur Praktische Chemie, , vol. 324, # 6 p. 1052 - 1054
