N-甲基-3-氧代-N-苯基丁酰胺合成路线 (共 9 条)
参考文献
Maiti, Arup; Reddy, P. V. Narasimha; Sturdy, Megan; Marler, Laura; Pegan, Scott D.; Mesecar, Andrew D.; Pezzuto, John M.; Cushman, Mark
Journal of Medicinal Chemistry, 2009 , vol. 52, # 7 p. 1873 - 1884
反应条件
Ru(bpy)3Cl2; triethylamine in N,N-dimethyl-formamide T=20°C; 12 h; Irradiation;
参考文献
Ju, Xuhui; Liang, Yan; Jia, Pingjing; Li, Weifei; Yu, Wei
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 3 p. 498 - 501
参考文献
Franich,R.A. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1972 , p. 2034 - 2041
反应条件
in anhydrous xylene 2 h; Reflux;
参考文献
Qi, Hengzhen; Yang, Zhanhui; Xu, Jiaxi
Synthesis, 2011 , # 5 p. 723 - 730
参考文献
Yuan, Yucheng; Yang, Rui; Zhang-Negrerie, Daisy; Wang, Junwei; Du, Yunfei; Zhao, Kang
Journal of Organic Chemistry, 2013 , vol. 78, # 11 p. 5385 - 5392
反应条件
sodium acetate Heating; Yield given. Title compound not separated from byproducts;
参考文献
Etkin, Nola; Babu, Suresh D.; Fooks, Catherine J.; Durst, Tony
Journal of Organic Chemistry, 1990 , vol. 55, # 3 p. 1093 - 1096
反应条件
PPA T=100°C; Cooling with ice;
参考文献
Maiti, Arup; Reddy, P. V. Narasimha; Sturdy, Megan; Marler, Laura; Pegan, Scott D.; Mesecar, Andrew D.; Pezzuto, John M.; Cushman, Mark
Journal of Medicinal Chemistry, 2009 , vol. 52, # 7 p. 1873 - 1884
反应条件
1: 86 percent / Et3N / acetonitrile / 14 h / Ambient temperature 2: 86 percent / rhodium(II)acetate / CH2Cl2 / 1 h / Ambient temperature; other N-aryldiazoacetamides and N-aryl-2-diazo-3-oxobutanamides; var. rhodium(II) compounds, Nafion-H, var. solvents, temp. and time 3: 86 percent / rhodium(II) acetate / CH2Cl2 / 1 h / Ambient temperature View Scheme
参考文献
Qi, Hengzhen; Yang, Zhanhui; Xu, Jiaxi
Synthesis, 2011 , # 5 p. 723 - 730
反应条件
1: 86 percent / Et3N / acetonitrile / 14 h / Ambient temperature
2: 86 percent / rhodium(II)acetate / CH2Cl2 / 1 h / Ambient temperature; other N-aryldiazoacetamides and N-aryl-2-diazo-3-oxobutanamides; var. rhodium(II) compounds, Nafion-H, var. solvents, temp. and time
View Scheme
参考文献
Qi, Hengzhen; Yang, Zhanhui; Xu, Jiaxi
Synthesis, 2011 , # 5 p. 723 - 730