N-邻苯二甲酰-L-谷氨酸酐合成路线 （共 17 条）
反应条件
1: tetrahydrofuran / 16 h / 20 °C 2: 43.8 g / hydrazine hydrate / ethanol / 4 h / Heating View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 36, # 2 p. 182 - 185
反应条件
1,4-dioxane; diethyl ether; ammonia
参考文献
King; Kidd
Journal of the Chemical Society, 1949 , p. 3315,3318
反应条件
1: 1.) pyridine, 2.) DCC / 1.) RT, overnight, 2.) 2 days 2: 89 percent / H2 / 10percent Pd/C / methanol / 2 h 3: 80 percent / bromoacetophenone, DMAP, Et3N / acetonitrile / 2 h / Ambient temperature View Scheme
参考文献
Robin, Sylvie; Zhu, Jiarong; Galons, Herve; Pham-Huy, Chuong; Claude, Jean Roger; et al.
Tetrahedron: Asymmetry, 1995 , vol. 6, # 6 p. 1249 - 1252
反应条件
1: 1.) BSTFA / 1.) CH3CN, 50 min, 2.) CH3CN 2: 2.0 M NH2NH2*H2O, Et3N / methanol; H2O 3: 1.) Hg(OAc)2, 2.) H2S (gas) / 1.) H2O, 38-41 deg C, 2.5 h, 2.) H2O, RT, 45 min View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 39, # 8 p. 1676 - 1681
反应条件
in 1,4-dioxane T=40°C; other time; Product distribution;
参考文献
Siewinski, Maciej; Kuropatwa, Marianna; Szewczuk, Apolinary
Analytical Chemistry, 1984 , vol. 56, p. 2882 - 2884
反应条件
1: methanol 2: ueber mehrere Stufen View Scheme
参考文献
DeWald; Moore
Journal of the American Chemical Society, 1958 , vol. 80, p. 3941,3943
反应条件
Behandeln des Reaktionsprodukts mit wss.NaHCO3 und anschliessend mit N2H4+H2O;
参考文献
Weygand; Reiher
Chemische Berichte, 1955 , vol. 88, p. 26,33
