1-[(4-硝基苯基)硫代]-2-丙酮合成路线 (共 5 条)
反应条件
triethylamine in methanol T=20°C; 1 h;
参考文献
G. D. Searle and Company
Patent: US6362183 B1, 2002 ;
Location in patent: Example 14 ;
US 6362183 B1
反应条件
potassium dihydrogenphosphate; tris-[2-carboxyethyl]-phosphine; human thiopurine S-methyltransferase; E. coli S-adenosylhomocysteine nucleosidase T=37°C; pH=8; Enzymatic reaction;
参考文献
Lee, Bobby W. K.; Sun, He G.; Zang, Tianzhu; Ju-Kim, Byung; Alfaro, Joshua F.; Zhou, Zhaohui Sunny
Journal of the American Chemical Society, 2010 , vol. 132, # 11 p. 3642 - 3643
参考文献
Zincke; Lenhardt
Justus Liebigs Annalen der Chemie, 1913 , vol. 400, p. 27
反应条件
potassium dihydrogenphosphate; tris-[2-carboxyethyl]-phosphine; human thiopurine S-methyltransferase; E. coli S-adenosylhomocysteine nucleosidase T=37°C; pH=8; Enzymatic reaction; Kinetics; Concentration;
参考文献
Lee, Bobby W. K.; Sun, He G.; Zang, Tianzhu; Ju-Kim, Byung; Alfaro, Joshua F.; Zhou, Zhaohui Sunny
Journal of the American Chemical Society, 2010 , vol. 132, # 11 p. 3642 - 3643
反应条件
PPA in chlorobenzene 5 h; Heating;
参考文献
Ple, Patrick A.; Marnett, Lawrence J.
Journal of Heterocyclic Chemistry, 1988 , vol. 25, p. 1271 - 1272