1-溴-4-(叔丁基磺酰基)苯合成路线 （共 17 条）
反应条件
aluminium trichloride T=20°C; 1 h;
参考文献
Pinault, Thomas; Cherioux, Frederic; Therrien, Bruno; Suess-Fink, Georg
Heteroatom Chemistry, 2004 , vol. 15, # 2 p. 121 - 126
反应条件
perchloric acid; acetic anhydride in acetic acid 3 h; cooling;
参考文献
Touaibia, Mohamed; Desjardins, Marc-Andre; Provencal, Alexandre; Audet, Daniel; Medard, Christelle; Morin, Mario; Breau, Livain
Synthesis, 2004 , # 14 p. 2283 - 2288
反应条件
pyridine; quinoline T=200°C;
参考文献
Journal of the American Chemical Society, , vol. 81, p. 4927,4929
反应条件
in dichloromethane; ethyl acetate
反应条件
(i) aq. H2SO4, (ii) /BRN= 507031/; Multistep reaction;
参考文献
Zhurnal Organicheskoi Khimii, , vol. 5, # 11 p. 2000 - 2005,1945 - 1949
反应条件
1: sodium periodate / water; methanol / 20 °C 2: 3-cyano-1-methylquinolinium perchlorate / acetonitrile-D3 / |Photolysis; |Schlenk technique View Scheme
参考文献
Cavattoni, Tullio; Del Giacco, Tiziana; Lanzalunga, Osvaldo; Mazzonna, Marco; Mencarelli, Paolo
Journal of Organic Chemistry, 2013 , vol. 78, # 10 p. 4886 - 4894
反应条件
1: 25 percent / PPh3 / trans-bis(triphenylphosphane)platinum(II) chloride / dimethylformamide / 16 h / 120 °C 2: 33 percent / Br2; AcOH / 20 °C View Scheme
参考文献
Blaszczyk, Alfred; Elbing, Mark; Mayor, Marcel
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 19 p. 2722 - 2724
反应条件
1: 4-(tert-butylsulfanyl)bromobenzene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.25 h; 2: N,N-dimethyl-formamide in tetrahydrofuran; water T=20°C; 0.5 h;
参考文献
Stuhr-Hansen, Nicolai; Christensen, Jorn B.; Harrit, Niels; Bjornholm, Thomas
Journal of Organic Chemistry, 2003 , vol. 68, # 4 p. 1275 - 1282
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane T=20°C;
参考文献
RESEARCH TRIANGLE INSTITUTE; THE REGENTS OF THE UNIVERSITY OF MICHIGAN; VIRGINIA COMMONWEALTH UNIVERSITY; CARROLL, Frank, Ivy; ONDACHI, Pauline, Wanjiku; NAVARRO, Hernan, A.; DAMAJ, M., Imad; WOODS, James, H.; JUTKIEWICZ, Emily, M.
Patent: WO2013/101802 A1, 2013 ;
Location in patent: Paragraph 0070; 0071; 0080; 0081 ;
反应条件
1: sodium periodate / water; methanol / 20 °C 2: 3-cyano-1-methylquinolinium perchlorate / acetonitrile-D3 / |Photolysis; |Schlenk technique View Scheme
参考文献
Cavattoni, Tullio; Del Giacco, Tiziana; Lanzalunga, Osvaldo; Mazzonna, Marco; Mencarelli, Paolo
Journal of Organic Chemistry, 2013 , vol. 78, # 10 p. 4886 - 4894
