1-(3-苯基丙-2-炔基)哌啶合成路线 (共 17 条)
反应条件
anhydrous iron chloride; N,N,N',N'-tetramethylguanidine in acetonitrile T=100°C; 12 h;
参考文献
Gao, Jian; Song, Qing-Wen; He, Liang-Nian; Yang, Zhen-Zhen; Dou, Xiao-Yong
Chemical Communications, 2012 , vol. 48, # 14 p. 2024 - 2026
反应条件
polymer-supported L-proline copper complex in dimethyl sulfoxide T=20°C; 2 h;
参考文献
Li, Qiang; Xie, Yun-Fu; Sun, Bao-Chuan; Yang, Jun; Song, Hai-Bin; Tang, Liang-Fu
Journal of Organometallic Chemistry, 2013 , vol. 745-746, p. 106 - 114
反应条件
formaldehyd in acetonitrile T=65°C; 3 h;
参考文献
Park, Kyungho; Heo, Yumi; Lee, Sunwoo
Organic Letters, 2013 , vol. 15, # 13 p. 3322 - 3325
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; cobalt(II) dibromide in acetonitrile T=80°C; Inert atmosphere;
参考文献
Tang, Yanchi; Xiao, Tiebo; Zhou, Lei
Tetrahedron Letters, 2012 , vol. 53, # 46 p. 6199 - 6201,3
反应条件
silver(I) acetate in 1,4-dioxane T=120°C; 10 h; Inert atmosphereSchlenk techniqueSealed tube;
参考文献
Chen, Xiuling; Chen, Tieqiao; Zhou, Yongbo; Au, Chak-Tong; Han, Li-Biao; Yin, Shuang-Feng
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 2 p. 247 - 250
反应条件
silver(I) acetate in 1,4-dioxane T=120°C; 12 h; Inert atmosphereSchlenk techniqueSealed tube;
参考文献
Chen, Xiuling; Chen, Tieqiao; Zhou, Yongbo; Au, Chak-Tong; Han, Li-Biao; Yin, Shuang-Feng
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 2 p. 247 - 250
反应条件
copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride T=20°C;
参考文献
Russo, Olivier; Messaoudi, Samir; Hamze, Abdallah; Olivi, Nathanaeel; Peyrat, Jean-Francois; Brion, Jean-Daniel; Sicsic, Sames; Berque-Bestel, Isabelle; Alami, Mouad
Tetrahedron, 2007 , vol. 63, # 43 p. 10671 - 10683
反应条件
benzoic acid in various solvent(s) T=90°C; 4 h;
参考文献
Kabalka, George W.; Venkataiah, Bollu; Dong, Gang
Tetrahedron Letters, 2004 , vol. 45, # 4 p. 729 - 731
反应条件
copper(II) bis(trifluoromethanesulfonate); copper(l) chloride in acetonitrile T=100°C; 12 h;
参考文献
Sakai, Norio; Uchida, Naoki; Konakahara, Takeo
Synlett, 2008 , # 10 p. 1515 - 1519
反应条件
N-bromosuccinmide; CuCl2·2H2O; sodium hydrogencarbonate in toluene T=20 - 110°C; 6 h; Inert atmosphere;
参考文献
Zhu, Yefeng; Zhao, Huishuang; Wei, Yunyang
Synthesis (Germany), 2013 , vol. 45, # 7 art. no. SS-2012-H0052-OP, p. 952 - 958