2-氯甲基-1,3-二氧戊环合成路线 (共 15 条)
反应条件
sulfonic group functionalized polyacrylonitrile preoxidated nanofiber mat in cyclohexane T=150°C; 2 h; Dean-Stark;
参考文献
Shao, Linjun; Xing, Guiying; He, Luyao; Chen, Ji; Xie, Hangqing; Liang, Xuezheng; Qi, Chenze
Applied Catalysis A: General, 2012 , vol. 443-444, p. 133 - 137
参考文献
Wu, Zhihong; Stanley, Roy R.; Pittman Jr., Charles U.
Journal of Organic Chemistry, 1999 , vol. 64, # 22 p. 8386 - 8395
反应条件
sodium carbonate in ethylene glycol
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 132, p. 970
Bulletin de la Societe Chimique de France, , vol. <3> 25, p. 585
反应条件
Unter vermindertem Druck;
参考文献
Journal of Organic Chemistry, , vol. 20, p. 178,179
反应条件
1,4-dioxane; platinum Hydrogenation;
参考文献
Chemische Berichte, , vol. 87, p. 1343,1350
反应条件
lithium aluminium tetrahydride; boron trichloride 1.) CH2Cl2, 0.2 h, 2.) Et2O, 30 min; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bonner, Trevor G.; Lewis, David; Rutter, Keith
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 1807 - 1810
反应条件
hydrogenchloride; acetone
参考文献
Astle; Pierce
Journal of Organic Chemistry, 1955 , vol. 20, p. 178,179
反应条件
lithium aluminium tetrahydride; boron trichloride 1.) CH2Cl2, 0.2 h, 2.) Et2O, 30 min; Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1807 - 1810
反应条件
lithium aluminium tetrahydride; boron trichloride 1.) CH2Cl2, 0.2 h, 2.) Et2O, 30 min; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1807 - 1810