N-苯甲酰-L-苯基丙氨酸合成路线 (共 71 条)
参考文献
Ducki, Sylvie; Hadfield, John A.; Zhang, Xiuguo; Lawrence, Nicholas J.; McGown, Alan T.
Planta Medica, 1996 , vol. 62, # 3 p. 277 - 278
反应条件
hydrogen; rhodium(I)-bis(1,5-cyclooctadiene) tetrafluoroborate; triethylamine; (R,R)-BICP in tetrahydrofuran T=20°C; P=750.075 Torr; 24 h;
参考文献
THE PENN STATE RESEARCH FOUNDATION
Patent: EP918781 B1, 2004 ;
Location in patent: Page 8 ;
反应条件
1: With water; sodium hydroxide in methanol 2: Acidic conditions;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 18, # 2 p. 887 - 895
反应条件
hydrogen; lt;Rh((S)-BINAP)gt;ClO4 in tetrahydrofuran P=3800 Torr; 48 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 40, # 8 p. 1245 - 1253
反应条件
hydrogen; triethylamine; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in ethanol; benzene 24 h; Ambient temperature;
参考文献
Yamashita, Mitsuji; Kobayashi, Mineaki; Sugiura, Motoyuki; Tsunekawa, Kenji; Oshikawa, Tatsuo; et al.
Bulletin of the Chemical Society of Japan, 1986 , vol. 59, # 1 p. 175 - 178
反应条件
trimethylaluminum in 1,2-dichloro-ethane T=80°C;
参考文献
Martin, Stephen F.; Dwyer, Michael P.; Lynch, Christopher L.
Tetrahedron Letters, 1998 , vol. 39, # 12 p. 1517 - 1520
反应条件
water in various solvent(s) T=50°C; 35 h;
参考文献
Journal of Organic Chemistry, , vol. 58, # 12 p. 3252 - 3258
反应条件
hydrogen; lt;(2R,3R)-2,3-Bis(diphenylphosphino)butangt;(π-norbornadien)rhodium(I)-perchlorate in tetrahydrofuran P=3000.2 Torr; 8 h; Yield given;
参考文献
Chemische Berichte, , vol. 113, # 6 p. 2323 - 2325
反应条件
D-amidase-substance from pseudomonas-cultures T=37°C;
参考文献
Nature (London, United Kingdom), , vol. 181, p. 1225
反应条件
hydrogen; lt;Rh(NBD)2gt;ClO4; (2R,3S)-1,2-bis(diphenylphosphino)-3-tBoc-aminobutane in ethanol 22 h; Ambient temperature; Yield given;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 33, # 4 p. 1342 - 1350