1H,1H,2H,2H,3H,3H-全氟-1-十一醇合成路线 （共 5 条）
反应条件
lithium aluminium tetrahydride in diethyl ether T=18°C; 16 h;
参考文献
Coe,P.L. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1975 , p. 654 - 656
反应条件
1: Cu / dimethylformamide / 56 h / 120 °C 2: dimethylformamide / 15 h / 110 °C 3: aq. H2SO4 / 15 h / 120 °C 4: H2 / Pd-C / ethanol / 15 h 5: LiAlH4 / diethyl ether / 16 h / 18 °C View Scheme
参考文献
Coe,P.L. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1975 , p. 654 - 656
反应条件
1: H2 / Pd-C / ethanol / 15 h 2: LiAlH4 / diethyl ether / 16 h / 18 °C View Scheme
参考文献
Coe,P.L. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1975 , p. 654 - 656
反应条件
1: dimethylformamide / 15 h / 110 °C 2: aq. H2SO4 / 15 h / 120 °C 3: H2 / Pd-C / ethanol / 15 h 4: LiAlH4 / diethyl ether / 16 h / 18 °C View Scheme
参考文献
Coe,P.L. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1975 , p. 654 - 656
反应条件
1: aq. H2SO4 / 15 h / 120 °C 2: H2 / Pd-C / ethanol / 15 h 3: LiAlH4 / diethyl ether / 16 h / 18 °C View Scheme
参考文献
Coe,P.L. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1975 , p. 654 - 656
