4-苄氧基-3-溴-5-甲氧基苯甲醛合成路线 （共 6 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide T=80°C; 4 h;
参考文献
Vanucci-Bacque, Corinne; Chaabouni, Slim; Fabing, Isabelle; Bedos-Belval, Florence; Baltas, Michel
Tetrahedron Letters, 2014 , vol. 55, # 2 p. 528 - 530
参考文献
Journal of the American Chemical Society, , vol. 71, p. 3851
反应条件
1.1: 21.1 g / Br2 / acetic acid / 0.17 h / 20 °C 2.1: n-Bu4NI; NaH / dimethylformamide / 0.17 h / 20 °C 2.2: 27.6 g / dimethylformamide / 20 °C View Scheme
参考文献
Organic letters, , vol. 3, # 17 p. 2661 - 2663
反应条件
1: (i) NH2OH*HCl, Py, (ii) DCC, CuSO4*5H2O, Et3N 2: H2 / Pd-C View Scheme
参考文献
Vowinkel,E.; Bartel,J.
Chemische Berichte, 1974 , vol. 107, p. 1221 - 1227
反应条件
tetrabutylammomium bromide; hydrogen bromide in dichloromethane 24 h; Heating;
参考文献
Bhalerao; Raju; Neelakantan
Synthetic Communications, 1995 , vol. 25, # 10 p. 1433 - 1439
反应条件
1.1: mCPBA / CH2Cl2 / 20 °C
1.2: 73 percent / KOH / methanol; H2O / 0.17 h / 20 °C
2.1: nBu4NI; NaH / dimethylformamide / 0.17 h / 20 °C
2.2: 83 percent / dimethylformamide / 20 °C
View Scheme
参考文献
Xie; Kozlowski
Organic letters, 2001 , vol. 3, # 17 p. 2661 - 2663
