2,4,6,8-四甲基-2,4,6,8-四乙烯基环四硅氧烷合成路线 （共 38 条）
反应条件
tetrabutyl ammonium fluoride; palladium (II) bromide; biphenyl-2-yl-di-tert-butyl-phosphane in tetrahydrofuran T=50°C; 2.5 h; Product distribution; Further Variations:ReagentsTemperaturesreaction times;
参考文献
Denmark, Scott E.; Butler, Christopher R.
Organic Letters, 2006 , vol. 8, # 1 p. 63 - 66
反应条件
tetrabutyl ammonium fluoride; palladium (II) bromide; biphenyl-2-yl-di-tert-butyl-phosphane in tetrahydrofuran T=50°C; 48 h;
参考文献
Denmark, Scott E.; Butler, Christopher R.
Organic Letters, 2006 , vol. 8, # 1 p. 63 - 66
反应条件
tetrabutyl ammonium fluoride; palladium (II) bromide; biphenyl-2-yl-di-tert-butyl-phosphane in tetrahydrofuran T=50°C; 3 h;
参考文献
Denmark, Scott E.; Butler, Christopher R.
Organic Letters, 2006 , vol. 8, # 1 p. 63 - 66
反应条件
Lewatit SPC 118 T=90°C; 4 h;
参考文献
Brand, Dagmar; Moretto, Hans-Heinrich; Schulze, Manfred; Wrobel, Dieter
Journal fuer Praktische Chemie/Chemiker-Zeitung, 1994 , vol. 336, # 3 p. 218 - 224
反应条件
1: D4v With tetrabutyl ammonium fluoride in tetrahydrofuran T=20°C; 0.166667 h; 2: 1-iodo-3-nitro-benzene With bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran T=20°C; 0.166667 h;
参考文献
Journal of Organometallic Chemistry, , vol. 624, # 1-2 p. 372 - 375
反应条件
1: D4v With triphenyl-arsane; tetrabutyl ammonium fluoride in tetrahydrofuran T=20°C; 0.166667 h; 2: 1-iodo-2-methoxybenzene With bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran T=20°C; 24 h;
参考文献
Denmark, Scott E.; Wang, Zhigang
Journal of Organometallic Chemistry, 2001 , vol. 624, # 1-2 p. 372 - 375
反应条件
tetrabutyl ammonium fluoride; palladium (II) bromide; biphenyl-2-yl-di-tert-butyl-phosphane in tetrahydrofuran T=50°C; 20 h;
参考文献
Denmark, Scott E.; Butler, Christopher R.
Organic Letters, 2006 , vol. 8, # 1 p. 63 - 66
反应条件
tetrabutyl ammonium fluoride; palladium (II) bromide; biphenyl-2-yl-di-tert-butyl-phosphane in tetrahydrofuran T=50°C; 24 h; Title compound not separated from byproducts;
参考文献
Denmark, Scott E.; Butler, Christopher R.
Organic Letters, 2006 , vol. 8, # 1 p. 63 - 66
反应条件
tetrabutyl ammonium fluoride; palladium (II) bromide; biphenyl-2-yl-di-tert-butyl-phosphane in tetrahydrofuran T=50°C; 5 h;
参考文献
Denmark, Scott E.; Butler, Christopher R.
Organic Letters, 2006 , vol. 8, # 1 p. 63 - 66
反应条件
tetrabutyl ammonium fluoride; palladium (II) bromide; biphenyl-2-yl-di-tert-butyl-phosphane in tetrahydrofuran
T=50°C; 4 h;
参考文献
Denmark, Scott E.; Butler, Christopher R.
Organic Letters, 2006 , vol. 8, # 1 p. 63 - 66
