1-(4-苯甲酰基-1-哌啶)-乙酮合成路线 （共 6 条）
反应条件
triethylamine in dichloromethane T=20°C; Inert atmosphere;
参考文献
US2014/107094 A1, ;
Paragraph 0635; 0636 ;
反应条件
1: SOCl2 / 1 h / 20 °C 2: AlCl3 / 1,2-dichloro-ethane / 2 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 46, # 25 p. 5512 - 5532
反应条件
aluminium trichloride in 1,2-dichloro-ethane Friedel-Crafts reaction; 2 h; Heating;
参考文献
Journal of Medicinal Chemistry, , vol. 46, # 25 p. 5512 - 5532
反应条件
hydrogenchloride Heating;
参考文献
Orjales, Aurelio; Mosquera, Ramon; Toledo, Antonio; Pumar, M. Carmen; Garcia, Neftali; Cortizo, Lourdes; Labeaga, Luis; Innerarity, Ana
Journal of Medicinal Chemistry, 2003 , vol. 46, # 25 p. 5512 - 5532
反应条件
1: aq. HCl / Heating 2: aq. NaHCO3 / 20 °C View Scheme
参考文献
Orjales, Aurelio; Mosquera, Ramon; Toledo, Antonio; Pumar, M. Carmen; Garcia, Neftali; Cortizo, Lourdes; Labeaga, Luis; Innerarity, Ana
Journal of Medicinal Chemistry, 2003 , vol. 46, # 25 p. 5512 - 5532
反应条件
1: aq. HCl / Heating
2: 89 percent / HCOOH / 3 h / 55 - 60 °C
3: 90 percent / NaBH4 / methanol; H2O / Heating
View Scheme
参考文献
Orjales, Aurelio; Mosquera, Ramon; Toledo, Antonio; Pumar, M. Carmen; Garcia, Neftali; Cortizo, Lourdes; Labeaga, Luis; Innerarity, Ana
Journal of Medicinal Chemistry, 2003 , vol. 46, # 25 p. 5512 - 5532
