(S)-(+)-1-茚醇合成路线 (共 57 条)
反应条件
lithium aluminium tetrahydride in tetrahydrofuran Ambient temperature;
参考文献
Boyd, Derek; Sharma, Narain D.; Smith, Alistair E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 11 p. 2767 - 2770
反应条件
50 U aminoacylase E.C. 3.5.1.14 in hexane Acetylation; 168 h;
参考文献
Bakker; Spruijt; Van Rantwijk; Sheldon
Tetrahedron Asymmetry, 2000 , vol. 11, # 8 p. 1801 - 1808
反应条件
Coprinus peroxidase; 2-methoxy-phenol in water T=20°C; 68 h; pH 7.0; Further byproducts given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 64, # 13 p. 4834 - 4839
反应条件
Lipase PS in di-isopropyl ether T=30°C; Esterification; 7 h; Enzymatic reaction; Title compound not separated from byproducts.;
参考文献
Journal of Organic Chemistry, , vol. 65, # 1 p. 83 - 88
反应条件
lipase Amano PS enzyme in di-isopropyl ether T=30°C; 7 h; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 37, # 41 p. 7369 - 7372
反应条件
lipase YS in di-isopropyl ether T=30°C; 7 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 10 p. 1253 - 1256
反应条件
lipase from Pseudomonas cepacia immobilized on ceramic in toluene T=40°C; 4 h;
参考文献
Monatshefte fur Chemie, , vol. 134, # 8 p. 1151 - 1157
反应条件
2: 97 percent / 0.1N KOH / ethanol / 18 h / 25 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 39, # 48 p. 8881 - 8884
反应条件
1: With C38H31Cl2N3O4PRe in 1,4-dioxane T=20°C; 2: With tetrabutyl ammonium fluoride in 1,4-dioxane T=20°C; optical yield given as percent eeenantioselective reaction;
参考文献
Chemistry - A European Journal, , vol. 16, # 31 p. 9555 - 9562
反应条件
immobilized Candida antarctica Lipase B in diethyl ether T=20°C; 24 h;
参考文献
Tetrahedron Asymmetry, , vol. 17, # 5 p. 797 - 800