1-羟基-3-甲基蒽-9,10-二酮合成路线 （共 22 条）
反应条件
Celite; silver carbonate; triethylamine in dichloromethane
0.0833333 h;
参考文献
Hauser, Frank M.; Takeuchi, Craig; Yin, Htwe; Corlett, Stephen A.
Journal of Organic Chemistry, 1994 , vol. 59, # 1 p. 258 - 259
反应条件
hydrogen bromide in acetic acid
3.5 h; Heating;
参考文献
Jung; Lowe III; Lyster; et al.
Tetrahedron, 1984 , vol. 40, # 22 p. 4751 - 4766
反应条件
sulfuric acid; boric acid
T=150°C;
参考文献
Steyermark; Gardner
Journal of the American Chemical Society, 1930 , vol. 52, p. 4884,4886
参考文献
Girex
Patent: US6057461 A1, 2000 ;
参考文献
Girex
Patent: US6057461 A1, 2000 ;
反应条件
1: 87 percent / LiAlH4, air / diethyl ether / 0.5 h / 25 °C
2: 18 percent / acetonitrile / 0.25 h / 25 °C
View Scheme
参考文献
Semmelhack; Ho, Suzzy; Cohen; Steigerwald; Lee; Gilbert, Adam M.; Wutff, William D.; Ball, Richard G.
Journal of the American Chemical Society, 1994 , vol. 116, # 16 p. 7108 - 7122
反应条件
2: 48 percent / NBS, benzoyl peroxide / CCl4 / 10.5 h / Heating
View Scheme
参考文献
Kraus; Cho; Crowley; et al.
Journal of Organic Chemistry, 1983 , vol. 48, # 20 p. 3439 - 3444
反应条件
1: 81 percent / LiO-t-Bu
2: 72 percent / N-bromosuccinimide / H2O; acetone / 1.) 0 deg C, 2.) from 0 deg C to room temp., 1 h
View Scheme
参考文献
Hauser, Frank M.; Prasanna, Subbarao
Journal of Organic Chemistry, 1982 , vol. 47, p. 383 - 384
反应条件
1: CH2Cl2 / 24 h / 20 °C
2: pyridinium chlorochromate, acetic acid / 5 h
View Scheme
参考文献
Krohn, Karsten; Klimars, Michael; Koehle, Hans-Juergen; Ebeling, Eckehardt
Tetrahedron, 1984 , vol. 40, # 19 p. 3677 - 3694
反应条件
1: 87 percent / 12 h / Heating
2: BuLi/i-Pr2NH / tetrahydrofuran / - 20 deg C, 30 min, then rt., 12 h
3: 2.) 5percent HCl / 1.) toluene, 80-100 deg C, 12 h; 2.) MeOH, rt., 10 h
View Scheme
参考文献
Khan; Blessing; Schmidt
Synthesis, 1994 , # 3 p. 255 - 257
