2,3-二苯基-1,3-丁二烯合成路线 （共 101 条）
反应条件
under N2; heating at 100°C for 1 h with stirring; filtered through silica gel (CDCl3); NMR;
参考文献
Powell, Kimberly R.; Elias, W. Jeff; Welker, Mark E.
Journal of Organometallic Chemistry, 1991 , vol. 407, # 1 p. 81 - 89
反应条件
1: S8 / pyridine / Heating
2: dimethylsulfoxide / 140 °C
View Scheme
参考文献
Rys, Andrzej Z.; Harpp, David N.
Tetrahedron Letters, 1997 , vol. 38, # 28 p. 4931 - 4934
反应条件
perchloric acid in tetrahydrofuran
T=55°C; 1.66667 h; Yield given. Yields of byproduct given;
参考文献
Ando, Wataru; Sonobe, Hideki; Akasaka, Takeshi
Tetrahedron, 1990 , vol. 46, # 15 p. 5093 - 5100
反应条件
1: sulfur / Reflux
2: Reflux
View Scheme
参考文献
Rys, Andrzej Z.; Schultz, Erwin K. V.; Harpp, David N.
Journal of Sulfur Chemistry, 2010 , vol. 31, # 5 p. 351 - 371
反应条件
(O2N-C6H4CH2SeS)2
4 h; Heating; Product distribution; Further Variations:Reagents;
参考文献
Rys, Andrzej Z.; Hou, Yihua; Abu-Yousef, Imad A.; Harpp, David N.
Tetrahedron Letters, 2004 , vol. 45, # 50 p. 9181 - 9184
参考文献
Mustafa
Journal of the American Chemical Society, 1949 , vol. 71, p. 1878
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Salkind; Mossunow
Zhurnal Obshchei Khimii, 1940 , vol. 10, p. 517,519
Chem. Zentralbl., 1940 , vol. 111, # II p. 1863
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Allen; Eliot; Bell
Canadian Journal of Research, Section B: Chemical Sciences, 1939 , vol. 17, p. 75,87
参考文献
Allen; Eliot; Bell
Canadian Journal of Research, Section B: Chemical Sciences, 1939 , vol. 17, p. 75,87
反应条件
sodium hydroxide; acetic acid in chloroform
参考文献
Energy Conversion Devices, Inc.
Patent: US4532078 A1, 1985 ;
反应条件
in chlorobenzene
byproducts: Ph2CCH2; at 80 °C; react. mechanism discussed;
参考文献
Koecher, Juergen; Neumann, Wilhelm P.
Organometallics, 1985 , vol. 4, p. 400 - 402
反应条件
in benzene
at 70-80 °C; excess of the butadiene applied; react. mechanism discussed; elem. anal.; 1H NMR spectrum; mass spectrum;
参考文献
Koecher, Juergen; Neumann, Wilhelm P.
Organometallics, 1985 , vol. 4, p. 400 - 402
