2,3-二苯基-1,3-丁二烯合成路线 （共 101 条）
反应条件
acetic anhydride
T=180 - 200°C;
参考文献
Thoerner; Zincke
Chemische Berichte, 1880 , vol. 13, p. 645
Full Text Show Details
Johlin
Journal of the American Chemical Society, 1917 , vol. 39, p. 292
反应条件
trifluoroacetic acid in dichloromethane
T=20°C; 1 h;
参考文献
Xi, Zhenfeng; Liu, Xiaozhong; Lu, Jianming; Bao, Fengyu; Fan, Hongtao; Li, Zhiping; Takahashi, Tamotsu
Journal of Organic Chemistry, 2004 , vol. 69, # 24 p. 8547 - 8549
反应条件
N,N'-diphenyl-1,4-benzoquinone-1,4-diimine in tetrahydrofuran
T=20°C; 0.5 h; Inert atmosphere;
参考文献
Amaya, Toru; Suzuki, Riyo; Hirao, Toshikazu
Chemistry - A European Journal, 2014 , vol. 20, # 3 p. 653 - 656
反应条件
sodium hydroxide; sodium tetrahydroborate; bis(thiophen-2-yl)ditelluride in methanol
Ambient temperature;
参考文献
Engman, Lars; Bystroem, Styrbjoern E.
Journal of Organic Chemistry, 1985 , vol. 50, # 17 p. 3170 - 3174
反应条件
1: bromobenzene With magnesium in tetrahydrofuran
T=60°C;
2: 2,3-dichloro-1,3-butadiene With [1,3-bis(diphenylphosphino) propane] dichloronickel(II) in tetrahydrofuran
T=20 - 50°C;
参考文献
Yamamoto, Takakazu; Yasuda, Takuma; Kobayashi, Kazuaki; Yamaguchi, Isao; Koizumi, Take-Aki; Ishii, Daisuke; Nakagawa, Masaru; Mashiko, Yoshihiro; Shimizu, Norihiro
Bulletin of the Chemical Society of Japan, 2006 , vol. 79, # 3 p. 498 - 500
反应条件
palladium diacetate; triphenylphosphine in tetrahydrofuran
T=65°C; Addition; Elimination; 4 h;
参考文献
Boehmer, Jutta; Grigg, Ronald
Tetrahedron, 1999 , vol. 55, # 47 p. 13463 - 13470
反应条件
1: 3,5-bis(trifluoromethyl)phenyl methyl sulfone With (Me2N)3P=NH in tetrahydrofuran
0.5 h;
2: benzil in tetrahydrofuran
T=0 - 20°C; Julia-Kocienski methylenation; 16 h;
参考文献
Alonso, Diego A.; Fuensanta, Monica; Najera, Carmen; Varea, Montserrat
Journal of Organic Chemistry, 2005 , vol. 70, # 16 p. 6404 - 6416
反应条件
potassium hydrogensulfate
参考文献
Alder; Haydn
Justus Liebigs Annalen der Chemie, 1950 , vol. 570, p. 201,208
反应条件
1: Methyltriphenylphosphonium bromide With n-butyllithium in tetrahydrofuran; Petroleum ether
T=0 - 20°C; 1 h;
2: benzil in tetrahydrofuran; Petroleum ether
Heating; Further stages.;
参考文献
Van Walree, Cornells A.; Van Der Wiel, Bas C.; Jenneskens, Leonardus W.; Lutz, Martin; Spek, Anthony L.; Havenith, Remco W. A.; Van Lenthe, Joop H.
European Journal of Organic Chemistry, 2007 , # 28 p. 4746 - 4751
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane) in diethyl ether
T=25°C;
参考文献
Fulcher; Hunter; Welker
Synthetic Communications, 1993 , vol. 23, # 2 p. 217 - 222
