N-(2,5-二溴苯基)乙酰胺合成路线 （共 9 条）
参考文献
Tour, James M.; Rawlett, Adam M.; Kozaki, Masatoshi; Yao, Yuxing; Jagessar, Raymond C.; Dirk, Shawn M.; Price, David W.; Reed, Mark A.; Zhou, Chong-Wu; Chen, Jia; Wang, Wenyong; Campbell, Ian
Chemistry - A European Journal, 2001 , vol. 7, # 23 p. 5118 - 5134
反应条件
pyridine 1 h; Reflux;
参考文献
Ci, Zhenhua; Yu, Xiaoqiang; Bao, Ming; Wang, Chaolei; Ma, Tingli
Dyes and Pigments, 2013 , vol. 96, # 3 p. 619 - 625
反应条件
1: 98 percent / sulfuric acid; nitric acid / CH2Cl2 / 1 h 2: SnCl2*2H2O / ethanol; tetrahydrofuran / 0.5 h 3: 27 g / Et3N / 1 h / 35 °C View Scheme
参考文献
Tour, James M.; Lamba, Jaydeep J. S.
Journal of the American Chemical Society, 1993 , vol. 115, # 11 p. 4935 - 4936
反应条件
1: SnCl2*2H2O / ethanol; tetrahydrofuran / 0.5 h 2: 27 g / Et3N / 1 h / 35 °C View Scheme
参考文献
Tour, James M.; Lamba, Jaydeep J. S.
Journal of the American Chemical Society, 1993 , vol. 115, # 11 p. 4935 - 4936
参考文献
Wheeler; Valentine
American Chemical Journal, 1899 , vol. 22, p. 273
反应条件
1: 29 percent / P4S10 / benzene / 18 h / Heating 2: 49 percent / N-methylpyrrolidinone, NaH / 1.5 h / 150 °C 3: 23 percent / N-bromosuccinimide, benzoyl peroxide / CCl4 / 14 h / Heating; Irradiation View Scheme
参考文献
Mylari; Larson; Beyer; Zembrowski; Aldinger; Dee; Siegel; Singleton
Journal of Medicinal Chemistry, 1991 , vol. 34, # 1 p. 108 - 122
反应条件
1: 63 percent / HNO3; H2SO4 / -20 - 20 °C 2: 88 percent / K2CO3 / CH2Cl2; methanol / 3 h View Scheme
参考文献
Kosynkin, Dmitry V.; Tour, James M.
Organic Letters, 2001 , vol. 3, # 7 p. 993 - 995
反应条件
sulfuric acid; nitric acid T=-5 - -3°C; 1 h;
参考文献
Wang, Changsheng; Batsanov, Andrei S.; Bryce, Martin R.; Sage, Ian
Synthesis, 2003 , # 13 p. 2089 - 2095
反应条件
1: 29 percent / P4S10 / benzene / 18 h / Heating 2: 49 percent / N-methylpyrrolidinone, NaH / 1.5 h / 150 °C View Scheme
参考文献
Mylari; Larson; Beyer; Zembrowski; Aldinger; Dee; Siegel; Singleton
Journal of Medicinal Chemistry, 1991 , vol. 34, # 1 p. 108 - 122
