2-(3-甲基-1H-1,2,4-噻唑-5-基)吡啶合成路线 （共 4 条）
反应条件
1: hydrazine / ethanol / 6 h / |Reflux 2: sodium hydroxide / N,N-dimethyl-formamide / 5 h / 0 - 25 °C / |Inert atmosphere 3: 0.08 h / 200 °C / |Inert atmosphere View Scheme
参考文献
Muller, Keven; Sun, Yu; Heimermann, Andreas; Menges, Fabian; Niedner-Schatteburg, Gereon; Van Wuellen, Christoph; Thiel, Werner R.
Chemistry - A European Journal, 2013 , vol. 19, # 24 p. 7825 - 7834
反应条件
1: sodium hydroxide / N,N-dimethyl-formamide / 5 h / 0 - 25 °C / |Inert atmosphere 2: 0.08 h / 200 °C / |Inert atmosphere View Scheme
参考文献
Muller, Keven; Sun, Yu; Heimermann, Andreas; Menges, Fabian; Niedner-Schatteburg, Gereon; Van Wuellen, Christoph; Thiel, Werner R.
Chemistry - A European Journal, 2013 , vol. 19, # 24 p. 7825 - 7834
反应条件
acetic anhydride T=20°C; 2 h;
参考文献
Zhen, Hongyu; Luo, Jie; Yang, Wei; Chen, Qiliang; Ying, Lei; Jianhua, Zou; Wu, Hongbin; Cao, Yong
Journal of Materials Chemistry, 2007 , vol. 17, # 27 p. 2824 - 2831
反应条件
sodium carbonate in tetrahydrofuran; N,N-dimethyl acetamide Inert atmosphere;
参考文献
Park, Hye Rim; Ha, Yunkyoung
Molecular Crystals and Liquid Crystals, 2011 , vol. 538, p. 67 - 74
