1-(2-氨基-5-甲基苯基)乙酮合成路线 （共 15 条）
反应条件
zirconium(IV) oxychloride T=160 - 180°C; 0.5 h;
参考文献
Ravi, Subban; Saravanan, Nagusamy; Shanthi, Andy; Dharmaraj, Nallusamy; Lakshmanan, Akoni J
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 4 p. 443 - 445
反应条件
1: With AlCl3, aluminium chloride; boron trichloride in n-heptane; toluene 2 h; Inert atmosphereReflux; 2: With hydrogenchloride; water in n-heptane; toluene T=20 - 80°C; 0.5 h; Inert atmosphere;
参考文献
Wang, Jingjing; Chen, Weiqiang; Zuo, Sujing; Liu, Lu; Zhang, Xinrui; Wang, Jianhui
Angewandte Chemie - International Edition, 2012 , vol. 51, # 49 p. 12334 - 12338
Angew. Chem., 2012 , vol. 124, # 49 p. 12500 - 12504,5
反应条件
1: With sulfuric acid T=0 - 20°C; 2 h; Inert atmosphereSchlenk technique; 2: With sodium hydrogencarbonate Inert atmosphereSchlenk technique;
参考文献
Bhanuchandra; Ramu Yadav; Rit, Raja K.; Rao Kuram, Malleswara; Sahoo, Akhila K.
Chemical Communications, 2013 , vol. 49, # 45 p. 5225 - 5227
反应条件
in tetrahydrofuran T=0°C; 6 h;
参考文献
Ren, Lei; Lian, Xiao-Lei; Gong, Liu-Zhu
Chemistry - A European Journal, 2013 , vol. 19, # 10 p. 3315 - 3318
反应条件
1: triethylamine / dichloromethane / 0 °C / Inert atmosphere 2: acetonitrile / 20 h / 20 °C / Inert atmosphere; UV-irradiation View Scheme
参考文献
Guerrini, Giacomo; Taddei, Maurizio; Ponticelli, Fabio
Journal of Organic Chemistry, 2011 , vol. 76, # 18 p. 7597 - 7601
参考文献
Ockenden; Schofield
Journal of the Chemical Society, 1953 , p. 612,616 1957 3175,3179
Full Text Show Details
Ardaschew; Minkin
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 1261; engl. Ausg. S. 1343
反应条件
hydrogenchloride; tin Heating;
参考文献
Doppler,T. et al.
Helvetica Chimica Acta, 1979 , vol. 62, p. 271 - 303
反应条件
1: (i) Mg, Et2O, (ii) /BRN= 2102443/, Et2O, (iii) aq. H2SO4, AcOH 2: Sn, aq. HCl / Heating View Scheme
参考文献
Doppler,T. et al.
Helvetica Chimica Acta, 1979 , vol. 62, p. 271 - 303
反应条件
1: Ozonolyse 2: aqueous HCl View Scheme
参考文献
Ockenden; Schofield
Journal of the Chemical Society, 1953 , p. 612,616 1957 3175,3179
反应条件
T=20 - 25°C; 24 h; Irradiationon silica gel; Yield given;
参考文献
Magdy, M.; Malik, Abdel-; Mayo, Paul de
Canadian Journal of Chemistry, 1984 , vol. 62, p. 1275 - 1278
