N,N-二甲基-2,2-二甲氧基乙酰胺合成路线 (共 2 条)
反应条件
sodium methylate in methanol T=0 - 75°C; Product distribution / selectivity;
参考文献
DSM FINE CHEMICALS AUSTRIA NFG GMBH and CO KG
Patent: WO2005/87711 A1, 2005 ;
Location in patent: Example 3; 10 ;
反应条件
1: in DMF (N,N-dimethyl-formamide)
T=60°C; 2 h; Heating;
2: With toluene-4-sulfonic acid in toluene
5 h; Heating / reflux;
参考文献
PFIZER LIMITED; PFIZER INC.
Patent: WO2005/28452 A1, 2005 ;
Location in patent: Page/Page column 59-60 ;
WO 2005/028452 A1