1-甲氧基-2-丙-2-基氧基苯合成路线 （共 14 条）
参考文献
SANOFI-AVENTIS
Patent: US2011/59955 A1, 2011 ;
Location in patent: Page/Page column 20 ;
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=100°C;
参考文献
Testaferri, L.; Tiecco, M.; Tingoli, M.; Chianelli, D.; Montanucci, M.
Tetrahedron, 1982 , vol. 38, # 24 p. 3687 - 3692
反应条件
potassium carbonate in dimethyl sulfoxide
参考文献
Pan, Yongchun; Peng, Zhonghua; Melinger, Joseph S.
Tetrahedron, 2003 , vol. 59, # 29 p. 5495 - 5506
反应条件
sodium hydroxide Heating;
参考文献
Siegman, John R.; Houser, John J.
Journal of Organic Chemistry, 1982 , vol. 47, # 14 p. 2773 - 2779
反应条件
trichlorophosphate T=100 - 115°C; Vilsmeier-Haack Formylation; 19 h; Cooling with ice; Overall yield = 84.4 percent; Overall yield = 6.5 g;
参考文献
Huang, Wei-Bin; Du, Cai-Yan; Jiang, Jian-An; Ji, Ya-Fei
Research on Chemical Intermediates, 2013 , vol. 39, # 6 p. 2849 - 2856
反应条件
sodium in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=100°C; 2 h;
参考文献
Testaferri, L.; Tiecco, M.; Tingoli, M.; Chianelli, D.; Montanucci, M.
Tetrahedron, 1982 , vol. 38, # 24 p. 3687 - 3692
参考文献
Birch
Journal of the Chemical Society, 1947 , p. 102,104
反应条件
1: trichlorophosphate / 19 h / 100 - 115 °C / |Cooling with ice 2: AlCl3, aluminium chloride / dichloromethane / 5 h / 20 °C View Scheme
参考文献
Huang, Wei-Bin; Du, Cai-Yan; Jiang, Jian-An; Ji, Ya-Fei
Research on Chemical Intermediates, 2013 , vol. 39, # 6 p. 2849 - 2856
参考文献
Acta Chimica Academiae Scientiarum Hungaricae, , vol. 12, p. 83,85, 89
反应条件
1: 93 percent / I2; HNO3; aq. H2SO4 / AcOH / CCl4 2: 92 percent / B-Br-9-BBN / CH2Cl2 / 1 h / Heating 3: Pd(PPh3)2Cl2; Et3N / dimethylformamide 4: TBAF / tetrahydrofuran View Scheme
参考文献
Pan, Yongchun; Peng, Zhonghua; Melinger, Joseph S.
Tetrahedron, 2003 , vol. 59, # 29 p. 5495 - 5506
