反应条件
1: vinyl acetate; (3aS,6aR)-hexahydrofuro[2,3-b]furan-3-ol in dichloromethane; tert-butyl methyl ether T=20°C; 5 h; Resolution of racemateLarge scale reactionEnzymatic reaction; 2: N,N'-disuccinimidyl-carbonate With triethylamine in acetonitrile T=20°C; 24 h; enantioselective reaction;
参考文献
Khmelnitsky, Yuri L.; Michels, Peter C.; Cotterill, Ian C.; Eissenstat, Michael; Sunku, Venkataiah; Veeramaneni, Venugopal R.; Cittineni, Hariprasad; Kotha, Gopal R.; Talasani, Shyamsunder R.; Ramanathan, Krishna K.; Chitineni, Vakula K.; Venepalli, Bhaskar R.
Organic Process Research and Development, 2011 , vol. 15, # 1 p. 279 - 283
