253185-03-4合成路线 （共 388 条）
反应条件
1: With sulfuric acid; acetic anhydride in acetic acid Electrolysis; 2: With potassium iodide in water
参考文献
Peacock; Pletcher
Tetrahedron Letters, 2000 , vol. 41, # 46 p. 8995 - 8998
反应条件
1: 1.) AlCl3, 3.) NaHCO3 2: 1 N aq. HCl / CH2Cl2 View Scheme
参考文献
Wadsworth, Donald H.; Geer, Susan M.; Detty, Michael R.
Journal of Organic Chemistry, 1987 , vol. 52, # 16 p. 3662 - 3668
反应条件
byproducts: isobutan, boron hydride; High Pressure; under N2; diborane and trihalogen-borane was added to t-butylbenzene at-130°C, then in a closed autoclave the mixture was heated to 130°C for 40 min; at -195.8°C H2 was removed, at room temp. the residue of trihalogen-borane and diborane were removed, unseparable isomers; elem. anal.;
参考文献
Paetzold, Peter; Hoffmann, Juergen
Chemische Berichte, 1980 , vol. 113, # 12 p. 3724 - 3733
反应条件
tri-tert-butyl phosphine; [bis(acetoxy)iodo]benzene; palladium diacetate T=100°C; 33 h; Inert atmosphereGlovebox; Overall yield = 4 percent;
参考文献
Shrestha, Ruja; Mukherjee, Paramita; Tan, Yichen; Litman, Zachary C.; Hartwig, John F.
Journal of the American Chemical Society, 2013 , vol. 135, # 23 p. 8480 - 8483
参考文献
Vertex Pharmaceuticals Incorported
Patent: US2011/98311 A1, 2011 ;
反应条件
trinitratooxovanadium(V) in dichloromethane 0.05 h; Ambient temperature;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 10 p. 1589 - 1590
反应条件
sulfuric acid; nitric acid 1 h;
参考文献
Kuhler; Fryklund; Bergman; Weilitz; Lee; Larsson
Journal of Medicinal Chemistry, 1995 , vol. 38, # 25 p. 4906 - 4916
反应条件
nitric acid T=50°C; 3 h;
参考文献
RSC Advances, , vol. 3, # 7 p. 2197 - 2202
反应条件
trinitratooxovanadium(V) in dichloromethane 0.05 h; Ambient temperature;
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 10 p. 1589 - 1590
参考文献
Neslon; Brown
Journal of the American Chemical Society, 1951 , vol. 73, p. 5605
