3-(异丁烯酰氧)丙基三甲氧基硅烷合成路线 （共 21 条）
反应条件
BiCl3 T=25°C; 72 h; Inert atmosphere;
参考文献
Waseda University; Dow Corning Toray Co., Ltd.; WAKABAYASHI, Ryutaro; KURODA, Kazuyuki; TANIGUCHI, Yoshinori; SUGIURA, Yasushi
Patent: WO2012/91154 A1, 2012 ;
Location in patent: Page/Page column 22; 24 ;
反应条件
4,4'-methylene-bis-(2,6-di-tert-butylphenol); tetra-n-butyl phosphonium chloride in acetone T=115°C; Purification / work up;
参考文献
Wacker-Chemie GmbH
Patent: EP1469002 A1, 2004 ;
Location in patent: Page 5 ;
反应条件
1,1-bis (3,5-di-t-butyl-4-hydroxyphenyl)-methane; tetra-n-butyl phosphonium chloride in acetone T=115°C; 4 h;
参考文献
US2004/171859 A1, ;
Page 3 ;
反应条件
N',N'-diphenyl-1,4-phenylenediamine; 2,6-di-tert-butyl-4-methyl-phenol; acetone; HPtCl6·6H2O T=75°C; P=18751.9 Torr; Inert atmosphere;
参考文献
US2010/179340 A1, ;
Page/Page column 6-7 ;
反应条件
1: ethylene,methyl methacrylate; trichlorosilane With ANTAGE STDP-N; bis(1,3-divinyl-1,1,3,3,-tetramethyldisiloxane)Pt(0) T=80°C; 2: methanol Product distribution / selectivity;
参考文献
DOW CORNING TORAY CO., LTD.
Patent: WO2007/20932 A1, 2007 ;
Location in patent: Page/Page column 11 ;
反应条件
hexaethylguanidinium chloride T=100°C; 3 h; Product distribution / selectivity;
参考文献
Sheridan, Robert E.; Divins, Larry A.; Powell, Michael R.
Patent: US2007/32673 A1, 2007 ;
Location in patent: Page/Page column 4 ;
反应条件
1: ethylene,methyl methacrylate With 2,6-di-tert-butyl-4-methyl-phenol; 1,3,5-trimethyl-2,4,6-tri-(3,5-di-tert-butyl-4-hydroxy-benzyl)-benzene; trichlorosilane; dihydrogen hexachloroplatinate in isopropyl alcohol; toluene 2: methanol With urea in isopropyl alcohol; toluene T=50°C;
参考文献
Sakai, Takashi; Hayashi, Kyoko; Yano, Fumika; Takami, Mie; Ino, Megumi; Korenaga, Toshinobu; Ema, Tadashi
Bulletin of the Chemical Society of Japan, 2003 , vol. 76, # 7 p. 1441 - 1446
反应条件
1: 2-methyl-2-propenoic acid With potassium hydroxide in toluene 2: (3-chloropropyl)trimethoxysilane With 4,4'-bismethylene(2,6-di-tert-butylphenol); tetra-n-butyl phosphonium chloride in toluene; butanone T=110°C; 4 h;
参考文献
Monatshefte fur Chemie, , vol. 134, # 8 p. 1081 - 1092
反应条件
T=22°C; Gas phase; Kinetics;
参考文献
Russian Journal of General Chemistry, , vol. 79, # 8 p. 1650 - 1655
