反应条件
1: With boron trifluoride diethyl etherate in tetrahydrofuran T=0°C; 0.25 h; Inert atmosphere; 2: With TMP2Mg*2LiCl in tetrahydrofuran T=-78°C; 0.0833333 h; Inert atmosphere; 3: With 1,2-dibromo-1,1,2,2-tetrachloroethane in tetrahydrofuran T=-78 - 25°C; Inert atmosphere; regioselective reaction;
参考文献
Klatt, Thomas; Roman, Daniela Sustac; Leon, Thierry; Knochel, Paul
Organic Letters, 2014 , vol. 16, # 4 p. 1232 - 1235