O,O-二乙基硫代磷酰氯合成路线 （共 132 条）
反应条件
potassium carbonate in acetonitrile 1.) 35 deg C, 1 h, 2.) 50 deg C, 4 h;
参考文献
Sapozhnikova, Zh. Z.; Prokof'eva, A. F.; Volkova, V. N.; Negrebetskii, V. V.; Prokovskaya, L. A.; Mel'nikov, N. N.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 2 p. 406 - 415,368 - 376
反应条件
potassium hydroxide; potassium carbonate; N,N,N',N,-tetramethylethylenediamine; N-benzyl-N,N,N-triethylammonium chloride in dichloromethane Ambient temperature;
参考文献
Petnehazy, Imre; Szakal, Gyoengyi; Toeke, Laszlo; Vida, Laszlo
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 9, p. 267 - 268
反应条件
potassium carbonate in acetonitrile 1.) 1 h, 35 deg C, 2.) 4 h, 50 deg C;
参考文献
Sapozhnikova, Zh. Z.; Prokof'eva, A. F.; Volkova, V. N.; Negrebetskii, V. V.; Prokovskaya, L. A.; Mel'nikov, N. N.
J. Gen. Chem. USSR (Engl. Transl.), 1991 , vol. 61, # 2 p. 406 - 415,368 - 376
反应条件
Petroleum ether und anschliessenden Erwaermen mit Schwefel;
参考文献
Arbusow et al.
Trudy Kazansk.Akad.Chem.Abstr., 1956 , # 2 p. 21,23,24
Trudy Kazansk.Akad.Chem.Abstr., 1957 , p. 10363
Full Text Show Details
Schrader
Ang.Ch.Monogr., 1952 , vol. 62, p. 44
参考文献
Arbusow et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1954 , p. 1038,1041;engl.Ausg.S.905
Chem.Abstr., 1957 , p. 10363
参考文献
McIvor et al.
Canadian Journal of Chemistry, 1956 , vol. 34, p. 1819,1827
反应条件
das Natrium-Salz reagiert;
参考文献
McIvor et al.
Canadian Journal of Chemistry, 1956 , vol. 34, p. 1819,1827
参考文献
Farbenfabr. Bayer
Patent: DE1026323 , 1955 ;
反应条件
1: (Z)-2-(2-aminothiazol-4-yl)-2-(triphenylmethoxyimino)acetic acid With tributyl-amine; 1,4-diaza-bicyclo[2.2.2]octane in dichloromethane T=20 - 30°C; 0.333333 h; Inert atmosphere; 2: O,O-diethyl chlorothiophosphate in dichloromethane T=2°C; 0.5 h;
参考文献
LONZA LTD; DAI, Danmei; ZHU, Wei; WANG, Siming
Patent: WO2011/29596 A1, 2011 ;
Location in patent: Page/Page column 8 ;
反应条件
in neat (no solvent) 20°C, 10-15 min; vac. distn. of reaction mixt.; confirmation by (1)H-NMR and IR spectroscopy;
参考文献
Journal of General Chemistry USSR (English Translation), , vol. 59, p. 2492 - 2493
Zhurnal Obshchei Khimii, , vol. 59, p. 2791 - 2792
