5-(溴甲基)-嘧啶 (8ci,9ci)合成路线 (共 2 条)
反应条件
N-bromosuccinmide in dichloromethane T=45°C; 48 h;
参考文献
Guo, Hongyan; Kim, Choung U.; Kim, Hae Soo; Lee, Chong-Kyo; Lee, Ill Young; Mitchell, Michael L.; Son, Jong Chan; Xu, Lianhong
Patent: US2008/70920 A1, 2008 ;
Location in patent: Page/Page column 106 ;
反应条件
1: With N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane 1 h; Heating / reflux; 2: With sodium hydrogencarbonate in tetrachloromethane; water
参考文献
Bradley, Paul Anthony; Dack, Kevin Neil; Marsh, Ian Roger
Patent: US2006/241125 A1, 2006 ;
Location in patent: Page/Page column 25 ;