3-(3,4,5-三甲氧基苯基)丙酸合成路线 (共 28 条)
反应条件
formic acid; palladium dichloride in sodium hydroxide; isopropyl alcohol 0.05 h; microwave irradiation;
参考文献
Sharma, Anuj; Joshi, Bhupendra P.; Sinha, Arun K.
Chemistry Letters, 2003 , vol. 32, # 12 p. 1186 - 1187
反应条件
5 Pd(II)/C(eggshell); hydrogen in tetrahydrofuran T=20°C; P=1551.49 Torr; 3 h;
参考文献
Shan, Shao-Jun; Zhang, Hong; Wang, Xiao-Dan
Journal of Chemical Research, 2012 , vol. 36, # 1 p. 56 - 57
反应条件
formic acid; triethylamine
反应条件
triethylammonium formate T=95 - 100°C; 72 h;
参考文献
Toth; Kover
Synthetic Communications, 1995 , vol. 25, # 19 p. 3067 - 3074
反应条件
1: 48 mg / hydrogen / Pd-C (10percent) / ethanol 2: 20percent aq. KOH / ethanol / 4 h / 100 °C View Scheme
参考文献
Phytochemistry (Elsevier), , vol. 24, # 11 p. 2589 - 2592
反应条件
1: 89 percent / piperidine / acetic acid / 0.03 h / microwave irradiation 2: 86 percent / PdCl2; formic acid / aq. NaOH; propan-2-ol / 0.05 h / microwave irradiation View Scheme
参考文献
Chemistry Letters, , vol. 32, # 12 p. 1186 - 1187
反应条件
potassium hydroxide in ethanol T=100°C; 4 h; Title compound not separated from byproducts;
参考文献
Phytochemistry (Elsevier), , vol. 24, # 11 p. 2589 - 2592
反应条件
morpholine; sulfur Erwaermen des Reaktionsprodukts mit aethanol. KOH;
参考文献
Journal of the American Chemical Society, , vol. 72, p. 4285
参考文献
Journal of the American Chemical Society, , vol. 75, p. 1889
参考文献
Monatshefte fuer Chemie, , vol. 90, p. 171,176