(3E)-3,7-辛二烯-2-酮合成路线 (共 9 条)
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in o-di-fluorobenzene; dimethyl sulfoxide T=80°C; 12 h;
参考文献
Nicolaou; Montagnon; Baran; Zhong
Journal of the American Chemical Society, 2002 , vol. 124, # 10 p. 2245 - 2258
反应条件
in tetrahydrofuran Wittig olefination; 12 h; Heating;
参考文献
Krafft, Marie E.; Haxell, Thomas F. N.
Journal of the American Chemical Society, 2005 , vol. 127, # 29 p. 10168 - 10169
反应条件
L-proline in chloroform Title compound not separated from byproducts;
参考文献
List; Pojarliev; Castello
Organic letters, 2001 , vol. 3, # 4 p. 573 - 575
反应条件
copper(l) chloride in diethyl ether 1.) 60 min 2.) -15 deg C, 30 min 3.) r.t., 1 h;
参考文献
Drouin, J.; Leyendecker, F.; Conia, J. M.
Tetrahedron, 1980 , vol. 36, # 82 p. 1195 - 1202
反应条件
1: pyridinium chlorochromate / dichloromethane / 1 h / 20 °C 2: dichloromethane / 24 h / |Reflux View Scheme
参考文献
Cui, Hai-Lei; Tanaka, Fujie
Chemistry - A European Journal, 2013 , vol. 19, # 20 p. 6213 - 6216
参考文献
Crandall,J.K.; Mayer,C.F.
Journal of Organic Chemistry, 1970 , vol. 35, # 9 p. 3049 - 3053
反应条件
(i) aq. Na2CO3, THF, (ii) CuO; Multistep reaction;
参考文献
Liedtke,R.J. et al.
Journal of Organic Chemistry, 1972 , vol. 37, p. 776 - 789
参考文献
Conia,J.-M.; le Pechec,P.
Tetrahedron Letters, 1965 , p. 3305 - 3311
参考文献
Castle, Lyle W.; Gross, M. L.
Organic Mass Spectrometry, 1989 , vol. 24, p. 637 - 646