3-溴噻吩[3,2-b]噻吩合成路线 （共 8 条）
反应条件
Amberlyst 15 in diethyl ether 10 h; Reflux;
参考文献
Henssler, John T.; Matzger, Adam J.
Organic Letters, 2009 , vol. 11, # 14 p. 3144 - 3147
反应条件
gold(I) chloride in 1,4-dioxane; water T=20°C; 3 h; Inert atmosphere;
参考文献
Yamamoto, Takuya; Katsuta, Hiroshi; Toyota, Kozo; Iwamoto, Takeaki; Morita, Noboru
Bulletin of the Chemical Society of Japan, 2012 , vol. 85, # 5 p. 613 - 623
参考文献
Tetrahedron Letters, , vol. 30, # 25 p. 3315 - 3318
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 43, # 1-2 p. 187 - 208
反应条件
1: POCl3 2: NaOEt 3: Cu / quinoline View Scheme
参考文献
Tetrahedron Letters, , vol. 30, # 25 p. 3315 - 3318
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 43, # 1-2 p. 187 - 208
反应条件
1: NaOEt 2: Cu / quinoline View Scheme
参考文献
Tetrahedron Letters, , vol. 30, # 25 p. 3315 - 3318
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 43, # 1-2 p. 187 - 208
反应条件
zinc in acetic acid 10 h; Heating;
参考文献
Journal of Heterocyclic Chemistry, , vol. 27, # 7 p. 2165 - 2173
反应条件
1.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 0 °C / Inert atmosphere 1.2: 16 h / -30 - 20 °C / Inert atmosphere 2.1: potassium carbonate / methanol / 12 h / 0 - 20 °C / Inert atmosphere 3.1: gold(I) chloride / 1,4-dioxane; water / 3 h / 20 °C / Inert atmosphere View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 85, # 5 p. 613 - 623
反应条件
1: potassium carbonate / methanol / 12 h / 0 - 20 °C / Inert atmosphere 2: gold(I) chloride / 1,4-dioxane; water / 3 h / 20 °C / Inert atmosphere View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 85, # 5 p. 613 - 623
