六氢-1H-氮杂卓-1-甲醛合成路线 （共 14 条）
反应条件
styrene; [Ru(η4-COD)(η3-methylallyl)2]; potassium tert-butylate; ICy*HCl in toluene T=125°C; 24 h; Inert atmosphereGlovebox;
参考文献
Ortega, Nuria; Richter, Christian; Glorius, Frank
Organic Letters, 2013 , vol. 15, # 7 p. 1776 - 1779
反应条件
sodium hydroxide; tetrabutyl ammonium fluoride T=50°C; 2 h;
参考文献
Gol'dberg, Yu. Sh.; Shimanskaya, M. V.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 10 p. 1789 - 1794
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 10 p. 2036 - 2042
反应条件
carbon monoxide; cobalt-magnesium oxide thorium oxide T=200°C; P=147102 Torr;
参考文献
Troyanskii, E. I.; Ioffe, V. A.; Nikishin, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, # 11 p. 2351 - 2359
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 11 p. 2537 - 2546
反应条件
sodium hydroxide; sodium peroxodisulphate; silver nitrate in water T=0°C; 2.5 h; Yields of byproduct given;
参考文献
Troyanskii, E. I.; Ioffe, V. A.; Nikishin, G. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, # 11 p. 2351 - 2359
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 11 p. 2537 - 2546
参考文献
Lovens Kemiske Fabrik Produktionsaktieselskab
Patent: US4554160 A1, 1985 ;
反应条件
in ethyl acetate 1 h; Ambient temperature;
参考文献
Neveux, Muriel; Bruneau, Christian; Dixneuf, Pierre H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 5 p. 1197 - 1199
参考文献
Leo Pharmaceutical Products Ltd. A/S
Patent: US4181659 A1, 1980 ;
反应条件
sodium hydroxide; sodium peroxodisulphate; silver nitrate in ammonium hydroxide; water 17 h; below 10 deg C;
参考文献
Ogawa, Keiichiro; Nomura, Yujiro; Takeuchi, Yoshito; Tomoda, Shuji
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , # 12 p. 3031 - 3036
反应条件
in diethyl ether T=25°C;
参考文献
Keiko, N. A.; Rulev, A. Yu.; Kalikhman, I. D.; Voronkov, M. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1987 , vol. 36, # 8 p. 1668 - 1671
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1987 , # 8 p. 1801 - 1805
反应条件
cyclopentanone 0.0666667 h; Heatingmicrowave irradiation;
参考文献
Torchy; Barbry
Journal of Chemical Research - Part S, 2001 , # 7 p. 292 - 293
