6-甲基吡啶-2-胺 1-氧化物合成路线 (共 11 条)
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in xylene 16 h; Heating;
参考文献
Chucholowski; Uhlendorf
Tetrahedron Letters, 1990 , vol. 31, # 14 p. 1949 - 1952
反应条件
1: pyridine 2: aqueous H2O2; acetic acid 4: aqueous HCl View Scheme
参考文献
Talbot, Eric P. A.; Richardson, Melodie; McKenna, Jeffrey M.; Toste, F. Dean
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 4 p. 687 - 691
参考文献
Brown
Journal of the American Chemical Society, 1957 , vol. 79, p. 3565
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Adams; Miyano
Journal of the American Chemical Society, 1954 , vol. 76, p. 2785
反应条件
1: acetic acid 2: aqueous NaOH View Scheme
参考文献
Adams; Miyano
Journal of the American Chemical Society, 1954 , vol. 76, p. 2785
参考文献
Katritzky
Journal of the Chemical Society, 1956 , p. 2063,2065
参考文献
Katritzky
Journal of the Chemical Society, 1956 , p. 2063,2065
反应条件
1: aqueous H2O2; acetic acid 3: aqueous HCl View Scheme
参考文献
Katritzky
Journal of the Chemical Society, 1956 , p. 2063,2065
反应条件
1: 2-amino-6-methylpyridine N-oxide With trifluoroacetic acid in dichloromethane 0.166667 h; 2: phenylacetylene With dichloro(pyridine-2-carboxylato)gold(III) in dichloromethane T=40°C; 22 h; regioselective reaction;
参考文献
Talbot, Eric P. A.; Richardson, Melodie; McKenna, Jeffrey M.; Toste, F. Dean
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 4 p. 687 - 691
反应条件
titanium tetrachloride; tin(ll) chloride in diethyl ether 0.5 h; Ambient temperature;
参考文献
Balicki, Roman; Kaczmarek, Lukasz; Malinowski, Marek
Synthetic Communications, 1989 , vol. 19, # 5and6 p. 897 - 900
反应条件
1: 60 percent / KI / dimethylformamide / 3 h / Heating
2: 54 percent / PCl3 / ethyl acetate / 3 h / Heating
View Scheme
参考文献
Kalinowski, Jerzy; Rykowski, Andrzej; Nantka-Namirski, Pawel
Polish Journal of Chemistry, 1984 , vol. 58, # 1-3 p. 125 - 134