2-甲氧基-5-甲基苯甲酸合成路线 (共 30 条)
反应条件
oxygen; palladium diacetate in acetic acid T=70°C; P=760.051 Torr; 15 h;
参考文献
Chemical Communications, , # 4 p. 486 - 488
反应条件
potassium hydroxide in methanol 2 h; Heating;
参考文献
Kahnberg, Pia; Lager, Erik; Rosenberg, Celia; Schougaard, Jette; Camet, Linda; Sterner, Olov; Nielsen, Elsebet stergaard; Nielsen, Mogens; Liljefors, Tommy
Journal of Medicinal Chemistry, 2002 , vol. 45, # 19 p. 4188 - 4201
反应条件
tetraethylammonium p-toluenesulfonate; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride in N,N-dimethyl-formamide Pt anode/Pt cathode; electrolysis with 2.5 mA/cm2;
参考文献
Torii, Sigeru; Tanaka, Hideo; Hamatani, Takeshi; Morisaki, Kazuo; Jutand, Anny; et al.
Chemistry Letters, 1986 , p. 169 - 172
反应条件
tert.-butylhydroperoxide; ruthenium(III) 1,4,7-triazacyclononane-based catalyst in dichloromethane; 1,2-dichloro-ethane T=20°C; 14 h;
参考文献
Cheung, Wai-Hung; Yip, Wing-Ping; Yu, Wing-Yiu; Che, Chi-Ming
Canadian Journal of Chemistry, 2005 , vol. 83, # 6-7 p. 521 - 526
反应条件
1: 10 percent Spectr. / tetranitromethane (TNM), tetrabutylammonium trinitromethide (TBAT) / acetonitrile / 7 h / 25 - 30 °C / Irradiation 2: cc. HCl / Ambient temperature View Scheme
参考文献
Journal of the American Chemical Society, , vol. 109, p. 7824
参考文献
Bulletin de la Societe Chimique de France, , vol. <4> 7, p. 334
反应条件
hydrogenchloride Ambient temperature;
参考文献
Journal of the American Chemical Society, , vol. 109, p. 7824
反应条件
1: 98 percent / K2CO3 / dimethylformamide / 20 h / 20 °C 2: 88 percent / 35percent aq. H2O2; 2M aq. KOH / methanol / 2 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 45, # 19 p. 4188 - 4201
反应条件
n-butyllithium; diethyl ether anschliessend mit CO2 behandeln;
参考文献
Journal of Organic Chemistry, , vol. 16, p. 869,872
反应条件
diethyl ether und Behandeln des Reaktionsloesung mit festem CO2;
参考文献
Journal of Organic Chemistry, , vol. 16, p. 869,872