3-[5-(环氧乙烷-2-基)戊基]十一烷酸甲酯合成路线 （共 11 条）
反应条件
chloro-trimethyl-silane; triethylamine in dichloromethane T=55°C;
参考文献
Rauf, Abdul; Ahmad, Shabana
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 8 p. 1924 - 1928
反应条件
Produkt5: 10-Oxo-octadecansaeure-methylester.Hydrogenation;
参考文献
Mack; Bickford
Journal of Organic Chemistry, 1953 , vol. 18, p. 686,691, 692
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Howton; Kaiser
Journal of Organic Chemistry, 1964 , vol. 29, p. 2420,2423
反应条件
potassium hydroxide; ethanol
参考文献
Gunstone; Jacobsberg
Chem. Physics Lipids, 1972 , vol. 9, p. 26,32
反应条件
chloro-trimethyl-silane; triethylamine in dichloromethane T=55°C;
参考文献
Rauf, Abdul; Ahmad, Shabana
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 8 p. 1924 - 1928
反应条件
Produkt5: 10-Oxo-octadecansaeure-methylester.Hydrogenation;
参考文献
Journal of Organic Chemistry, , vol. 18, p. 686,691, 692
Journal of Organic Chemistry, , vol. 29, p. 2420,2423
反应条件
1: With 2-mercaptobenzothiazole; triethylamine T=90°C; 24 h; 2: With KHSO5*0.5KHSO4*0.5K2SO4; sodium hydrogencarbonate in water; acetone T=0°C; 24 h; 3: With 1,8-diazabicyclo[5.4.0]undec-7-ene in methanol T=20°C; 1 h; Inert atmosphere; stereospecific reaction;
参考文献
European Journal of Organic Chemistry, , # 10 p. 1989 - 1998
反应条件
Tris(phenylseleno)borane; sodium hydrogencarbonate 1.) chloroform, 20 deg C, 49 h; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 22, # 26 p. 2491 - 2494
反应条件
Tris(methylseleno)borane; sodium hydrogencarbonate 1.) chloroform, 20 deg C, 54 h; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 22, # 26 p. 2491 - 2494
反应条件
sodium hydrogencarbonate 1.) chloroform, 20 deg C, 3 h; Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 22, # 26 p. 2491 - 2494
反应条件
Produkt5: 10-Oxo-octadecansaeure-methylester.Hydrogenation;
参考文献
Mack; Bickford
Journal of Organic Chemistry, 1953 , vol. 18, p. 686,691, 692
Full Text View citing articles Show Details
Howton; Kaiser
Journal of Organic Chemistry, 1964 , vol. 29, p. 2420,2423
