(2E)-2-癸烯-1-基乙酸酯合成路线 （共 19 条）
反应条件
in N,N-dimethyl-formamide 12 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Martinez, Antonio Garcia; Villalobos, Angeles Cruces; Ruiz, Manuel Oliver
Synthesis, 1988 , # 1 p. 58 - 60
反应条件
1: diethyl ether 2: pyridine; PBr3 3: glacial acetic acid View Scheme
参考文献
Delaby
Bulletin de la Societe Chimique de France, 1936 , vol. <5>3, p. 2380
反应条件
(bipyrimidine)Pd(OAc)2; p-benozquinone T=70°C; 20 h;
参考文献
Lin, Bo-Lin; Labinger, Jay A.; Bercaw, John E.
Canadian Journal of Chemistry, 2009 , vol. 87, # 1 SPEC. ISS. p. 264 - 271
参考文献
Delaby
Bulletin de la Societe Chimique de France, 1936 , vol. <5>3, p. 2380
反应条件
sodium acetate 1.) CH3COOH, room temp., 2.) CH3COOH, 170 deg C, 3 d; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Garcia Martinez, Antonio; Oliver Ruiz, Manuel; Contelles, Jose Luis Marco
Synthesis, 1986 , # 1 p. 125 - 128
反应条件
sodium tetrahydroborate; RuCl3*xH2O in N-methyl-formamide; water T=0°C; 1 h;
参考文献
Babler, James H.; White, Nicholas A.; Kowalski, Eric; Jast, Jeffrey R.
Tetrahedron Letters, 2011 , vol. 52, # 7 p. 745 - 748
反应条件
sodium cyanoborohydride; triphenylphosphine; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=25°C; 24 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Hutchins, Robert O.; Learn, Keith; Fulton, Robert P.
Tetrahedron Letters, 1980 , vol. 21, p. 27 - 30
反应条件
sodium tetrahydroborate; RuCl3*xH2O in N-methyl-formamide; water T=0°C; 1 h;
参考文献
Babler, James H.; White, Nicholas A.; Kowalski, Eric; Jast, Jeffrey R.
Tetrahedron Letters, 2011 , vol. 52, # 7 p. 745 - 748
反应条件
sodium cyanoborohydride; triphenylphosphine; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=25°C; 24 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Hutchins, Robert O.; Learn, Keith; Fulton, Robert P.
Tetrahedron Letters, 1980 , vol. 21, p. 27 - 30
