4-甲基苯磺酸-4-碘苯酯合成路线 （共 5 条）
反应条件
pyridine in dichloromethane T=0 - 20°C; 4 h;
参考文献
Xu, Song; Chen, Huan-Huan; Dai, Jian-Jun; Xu, Hua-Jian
Organic Letters, 2014 , vol. 16, # 9 p. 2306 - 2309
反应条件
in tetrahydrofuran T=110°C; Inert atmosphere; Overall yield = 59 percent; Overall yield = 50 mg;
参考文献
Minami, Hiroki; Wang, Xuan; Wang, Chao; Uchiyama, Masanobu
European Journal of Organic Chemistry, 2013 , # 35 p. 7891 - 7894
反应条件
dichloro(cycloocta-1,5-diene)palladium(II); N,N-dicyclohexylmethylamine; potassium formiate; tetra-(n-butyl)ammonium iodide; PCy3∙HBF4; bis(dibenzylideneacetone)-palladium(0); [(t-Bu)3PH]BF4 in acetonitrile
T=80°C; 18 h; Sealed tubeGloveboxInert atmosphere; Reagent/catalystSolvent;
参考文献
Korsager, Signe; Taaning, Rolf H.; Lindhardt, Anders T.; Skrydstrup, Troels
Journal of Organic Chemistry, 2013 , vol. 78, # 12 p. 6112 - 6120
反应条件
dichloro(cycloocta-1,5-diene)palladium(II); t-Bu Brett Phos; N,N-dicyclohexylmethylamine; COgen; bis(dibenzylideneacetone)-palladium(0); [(t-Bu)3PH]BF4 in 1,4-dioxane
T=80°C; 18 h; Inert atmosphere; Reagent/catalyst;
参考文献
Korsager, Signe; Taaning, Rolf H.; Skrydstrup, Troels
Journal of the American Chemical Society, 2013 , vol. 135, # 8 p. 2891 - 2894
反应条件
dichloro(cycloocta-1,5-diene)palladium(II); N,N-dicyclohexylmethylamine; 1,5-bis-(diphenylphosphino)-pentane; COgen; bis(dibenzylideneacetone)-palladium(0); [(t-Bu)3PH]BF4 in 1,4-dioxane
T=80°C; 18 h; Inert atmosphere; Reagent/catalyst;
参考文献
Korsager, Signe; Taaning, Rolf H.; Skrydstrup, Troels
Journal of the American Chemical Society, 2013 , vol. 135, # 8 p. 2891 - 2894
