N-[2-(3,4-二羟基苯基)乙基]乙酰胺合成路线 （共 10 条）
反应条件
triethylamine in acetonitrile T=20°C; 1 h;
参考文献
Jai, Woong Seo; Srisook, Ekaruth; Hyo, Jin Son; Hwang, Onyou; Cha, Young-Nam; Dae, Yoon Chi
Bioorganic and Medicinal Chemistry Letters, 2005 , vol. 15, # 14 p. 3369 - 3373
反应条件
boron tribromide in dichloromethane T=0 - 20°C; 20 h;
参考文献
Fong, Hugo K.H.; Copp, Brent R.
Marine Drugs, 2013 , vol. 11, # 2 p. 274 - 299
反应条件
sodium acetate in N,N-dimethyl-formamide 4.5 h; Ambient temperature;
参考文献
Cambie, Richard C.; Clark, George R.; Coombe, Sheryl L.; Coulson, Sally A.; Rutledge, Peter S.; Woodgate, Paul D.
Journal of Organometallic Chemistry, 1996 , vol. 507, # 1-2 p. 1 - 21
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane Acetylation;
参考文献
Ketuly, Kamal Aziz; Hadi, A. Hamid A.
Molecules, 2010 , vol. 15, # 4 p. 2347 - 2356
反应条件
1: triethylamine / 1 h / 20 °C / |Inert atmosphere 2: boron tribromide / dichloromethane / 20 h / 0 - 20 °C View Scheme
参考文献
Fong, Hugo K.H.; Copp, Brent R.
Marine Drugs, 2013 , vol. 11, # 2 p. 274 - 299
反应条件
hydrogenchloride T=40°C; 1 h;
参考文献
Andersen; Jacobsen; Roepstorff
Tetrahedron, 1980 , vol. 36, # 22 p. 3249 - 3252
反应条件
1: Locusta migratoria, Na2EDTA, O2 / Ambient temperature; 0.2M Na-acetate buffer, pH 5.5, overnight incubation 2: 6M HCl / 3 h / 110 °C View Scheme
参考文献
Andersen; Jacobsen; Roepstorff
Tetrahedron, 1980 , vol. 36, # 22 p. 3249 - 3252
反应条件
1: Locusta migratoria, Na2EDTA, O2 / Ambient temperature; 0.2M Na-acetate buffer, pH 5.5, overnight incubation 2: 6M HCl / 3 h / 110 °C View Scheme
参考文献
Andersen; Jacobsen; Roepstorff
Tetrahedron, 1980 , vol. 36, # 22 p. 3249 - 3252
反应条件
1: Locusta migratoria, Na2EDTA, O2 / Ambient temperature; 0.2M Na-acetate buffer, pH 5.5, overnight incubation 2: conc HCl / 1 h / 40 °C View Scheme
参考文献
Andersen; Jacobsen; Roepstorff
Tetrahedron, 1980 , vol. 36, # 22 p. 3249 - 3252
反应条件
1: Locusta migratoria, Na2EDTA, O2 / Ambient temperature; 0.2M Na-acetate buffer, pH 5.5, overnight incubation
2: 6M HCl / 3 h / 110 °C
View Scheme
参考文献
Andersen; Jacobsen; Roepstorff
Tetrahedron, 1980 , vol. 36, # 22 p. 3249 - 3252
