(E)-4-氧代己-2-烯醛合成路线 (共 3 条)
反应条件
bromine; sodium carbonate in methanol; diethyl ether
参考文献
Gollnick, Klaus; Griesbeck, Axel
Tetrahedron, 1985 , vol. 41, # 11 p. 2057 - 2068
反应条件
triphenylphosphine in Petroleum ether; benzene T=0°C; 1 h;
参考文献
Gollnick, Klaus; Griesbeck, Axel
Tetrahedron, 1985 , vol. 41, # 11 p. 2057 - 2068
反应条件
n-butyllithium 1.) ether, -40 - -50 deg C, 15 min, 2.) reflux, 2 h; Yield given. Multistep reaction;
参考文献
Mavrov, M. V.; Simirskaya, N. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 3 p. 595 - 596
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 3 p. 657 - 658