4-硝基-4-二甲基氨基偶氮苯合成路线 （共 38 条）
反应条件
1: 4-nitro-aniline With hydrogenchloride; sodium nitrite in water 1 h; Cooling with ice; 2: N,N-dimethyl-aniline With hydrogenchloride in water T=0 - 5°C; 2 h;
参考文献
Miao, Shifeng; Li, Hua; Xu, Qingfeng; Li, Najun; Zheng, Junwei; Sun, Ru; Lu, Jianmei; Li, Chang Ming
Journal of Materials Chemistry, 2012 , vol. 22, # 32 p. 16582 - 16589
反应条件
sodium hydroxide in water T=0 - 5°C; pH=6 - 7; 0.333333 h;
参考文献
Valizadeh, Hassan; Amiri, Mohammad; Hosseinzadeh, Fatemeh
Dyes and Pigments, 2012 , vol. 92, # 3 p. 1308 - 1313
反应条件
in ethanol; water T=8°C; 2 h;
参考文献
Colonna, Martino; Greci, Lucedio; Poloni, Marino
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 455 - 460
反应条件
in ethanol; water T=8°C; 3 h;
参考文献
Colonna, Martino; Greci, Lucedio; Poloni, Marino
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 455 - 460
反应条件
in ethanol; water T=8°C; 3 h;
参考文献
Colonna, Martino; Greci, Lucedio; Poloni, Marino
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 455 - 460
反应条件
in ethanol; water T=8°C; 3 h;
参考文献
Colonna, Martino; Greci, Lucedio; Poloni, Marino
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 455 - 460
反应条件
1: hydrogenchloride / water / 0.67 h / 0 - 5 °C 2: sodium hydroxide / water / 0.33 h / 0 - 5 °C / pH 6 - 7 View Scheme
参考文献
Dyes and Pigments, , vol. 92, # 3 p. 1308 - 1313
反应条件
in ethanol; water T=8°C; 3 h;
参考文献
Colonna, Martino; Greci, Lucedio; Poloni, Marino
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1982 , p. 455 - 460
反应条件
1: aq. HCl / diazotization 2: 5N aq. HCl/NaOAc View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , p. 947 - 953
Zhurnal Organicheskoi Khimii, , vol. 22, # 5 p. 1054 - 1061
反应条件
in ethanol; water T=8°C; 6 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 455 - 460
