2,4,6-三甲基苯磺酸叠氮化物合成路线 (共 5 条)
反应条件
1: With trichloroisocyanuric acid; triphenylphosphine in tetrahydrofuran T=0 - 5°C; 2: With sodium azide in tetrahydrofuran T=5 - 20°C; 0.0666667 h;
参考文献
Kiani, Adeleh; Akhlaghinia, Batool; Rouhi-Saadabad, Hamed; Bakavoli, Mehdi
Journal of Sulfur Chemistry, 2014 , vol. 35, # 2 p. 119 - 127
反应条件
sodium azide in ethanol T=25°C; 0.2 h;
参考文献
Jafarpour, Maasoumeh; Rezaeifard, Abdolreza; Golshani, Tayebeh
Phosphorus, Sulfur and Silicon and the Related Elements, 2011 , vol. 186, # 1 p. 140 - 148
反应条件
trifluoromethanesulfonyl azide; sodium hydrogencarbonate; copper(II) sulfate in water; toluene; tert-butyl alcohol T=20°C; 40 h;
参考文献
Raushel, Jessica; Pitram, Suresh M.; Fokin, Valery V.
Organic Letters, 2008 , vol. 10, # 16 p. 3385 - 3388
反应条件
copper(l) chloride in methanol T=20°C; Chan-Lam Coupling; 2 h;
参考文献
Moon, Soo-Yeon; Nam, Jungsoo; Rathwell, Kris; Kim, Won-Suk
Organic Letters, 2014 , vol. 16, # 2 p. 338 - 341
参考文献
Abramovitch,R.A. et al.
Journal of Organic Chemistry, 1977 , vol. 42, p. 2920 - 2926