2-(3-丁烯-1-基)萘合成路线 （共 18 条）
反应条件
potassium-sodium in tetrahydrofuran
Ambient temperature; Further byproducts given;
参考文献
Thornton, Todd A.; Ross, Gerald A.; Patil, Dilip; Mukaida, Kenichi; Warwick, Jeffrey O.; et al.
Journal of the American Chemical Society, 1989 , vol. 111, # 7 p. 2434 - 2440
反应条件
potassium-sodium in tetrahydrofuran
Ambient temperature; Further byproducts given;
参考文献
Thornton, Todd A.; Ross, Gerald A.; Patil, Dilip; Mukaida, Kenichi; Warwick, Jeffrey O.; et al.
Journal of the American Chemical Society, 1989 , vol. 111, # 7 p. 2434 - 2440
反应条件
potassium-sodium in tetrahydrofuran
Ambient temperature; Further byproducts given;
参考文献
Thornton, Todd A.; Ross, Gerald A.; Patil, Dilip; Mukaida, Kenichi; Warwick, Jeffrey O.; et al.
Journal of the American Chemical Society, 1989 , vol. 111, # 7 p. 2434 - 2440
反应条件
1.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere
1.2: 0 - 20 °C / Inert atmosphere
2.1: InOTf / dichloromethane / 14 h / 25 °C / Inert atmosphere
View Scheme
参考文献
Dao, Hai Thanh; Schneider, Uwe; Kobayashi, Shu
Chemical Communications, 2011 , vol. 47, # 2 p. 692 - 694
反应条件
in tetrahydrofuran
12 h; Heating; Yield given;
参考文献
Thornton, Todd A.; Ross, Gerald A.; Patil, Dilip; Mukaida, Kenichi; Warwick, Jeffrey O.; et al.
Journal of the American Chemical Society, 1989 , vol. 111, # 7 p. 2434 - 2440
反应条件
1: 4,4,5,5-tetramethyl-2-(naphthalen-2-yl)-1,3,2-dioxaborolane With tert.-butyl lithium in tetrahydrofuran; pentane
T=-78 - 0°C; 1 h; Inert atmosphere;
2: bromomethyl-cyclopropane With FeCl2(TMS-SciOPP); magnesium bromide in tetrahydrofuran
T=40°C; Suzuki-Miyaura coupling; 3 h; Inert atmosphere;
参考文献
Hatakeyama, Takuji; Hashimoto, Toru; Kondo, Yoshiyuki; Fujiwara, Yuichi; Seike, Hirofumi; Takaya, Hikaru; Tamada, Yoshinori; Ono, Teruo; Nakamura, Masaharu
Journal of the American Chemical Society, 2010 , vol. 132, # 31 p. 10674 - 10676
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene
16 h; Heating; Yield given. Yields of byproduct given;
参考文献
Abeywickrema, Anil N.; Beckwith, Athelstan L. J.; Gerba, Sendaba
Journal of Organic Chemistry, 1987 , vol. 52, # 18 p. 4072 - 4078
反应条件
in N,N-dimethyl-formamide
Hg, TBAP, -2.5 V vs SCE; other electrode, addition of D2O or sodium isopropylate; Product distribution;
参考文献
Thornton, Todd A.; Ross, Gerald A.; Patil, Dilip; Mukaida, Kenichi; Warwick, Jeffrey O.; et al.
Journal of the American Chemical Society, 1989 , vol. 111, # 7 p. 2434 - 2440
