2-(3-丁烯-1-基)萘合成路线 （共 18 条）
反应条件
in diethyl ether
T=0 - 23°C; 14 h;
参考文献
Waser, Jerome; Nambu, Hisanori; Carreira, Erick M.
Journal of the American Chemical Society, 2005 , vol. 127, # 23 p. 8294 - 8295
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Waser, Jerome; Gaspar, Boris; Nambu, Hisanori; Carreira, Erick M.
Journal of the American Chemical Society, 2006 , vol. 128, # 35 p. 11693 - 11712
反应条件
n-butyllithium in diethyl ether
1.) -78 deg C, 2 h, 2.) 23 deg C, 28 h; Yields of byproduct given;
参考文献
Thornton, Todd A.; Ross, Gerald A.; Patil, Dilip; Mukaida, Kenichi; Warwick, Jeffrey O.; et al.
Journal of the American Chemical Society, 1989 , vol. 111, # 7 p. 2434 - 2440
反应条件
InOTf in dichloromethane
T=25°C; 14 h; Inert atmosphere;
参考文献
Dao, Hai Thanh; Schneider, Uwe; Kobayashi, Shu
Chemistry - An Asian Journal, 2011 , vol. 6, # 9 p. 2522 - 2529
反应条件
anhydrous iron chloride in 1,2-dichloro-ethane
T=20°C; 2 h; chemoselective reaction;
参考文献
Chan, Li Yan; Lim, Jazreel Seh Kai; Kim, Sunggak
Synlett, 2011 , # 19 art. no. U05811ST, p. 2862 - 2866
反应条件
1: in tetrahydrofuran
T=20°C; 0.5 h; Inert atmosphere;
2: With phosphonic acid diethyl ester in tetrahydrofuran
Inert atmosphere;
参考文献
Li, Ying; Hu, Yuan-Yuan; Zhang, Song-Lin
Chemical Communications, 2013 , vol. 49, # 90 p. 10635 - 10637
反应条件
1: 64 percent / diethyl ether / 48 h / Ambient temperature
2: Bu3SnH, AIBN / benzene / 16 h / Heating
View Scheme
参考文献
Abeywickrema, Anil N.; Beckwith, Athelstan L. J.; Gerba, Sendaba
Journal of Organic Chemistry, 1987 , vol. 52, # 18 p. 4072 - 4078
反应条件
1: 59 percent / N-bromosuccinimide
2: 64 percent / diethyl ether / 48 h / Ambient temperature
3: Bu3SnH, AIBN / benzene / 16 h / Heating
View Scheme
参考文献
Abeywickrema, Anil N.; Beckwith, Athelstan L. J.; Gerba, Sendaba
Journal of Organic Chemistry, 1987 , vol. 52, # 18 p. 4072 - 4078
反应条件
1: tetrahydrofuran / 12 h / Heating
2: Na-K / tetrahydrofuran; various solvent(s) / Ambient temperature
View Scheme
参考文献
Thornton, Todd A.; Ross, Gerald A.; Patil, Dilip; Mukaida, Kenichi; Warwick, Jeffrey O.; et al.
Journal of the American Chemical Society, 1989 , vol. 111, # 7 p. 2434 - 2440
反应条件
1: N-bromosuccimide, benzoyl peroxide / CCl4 / 168 h / Heating
2: tetrahydrofuran / 12 h / Heating
View Scheme
参考文献
Thornton, Todd A.; Ross, Gerald A.; Patil, Dilip; Mukaida, Kenichi; Warwick, Jeffrey O.; et al.
Journal of the American Chemical Society, 1989 , vol. 111, # 7 p. 2434 - 2440
反应条件
1: C15H16O With Co(3-Me-5-MeO-salen) in acetonitrile
T=-20 - 20°C; 0.166667 h; Inert atmosphere;
2: 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical With dihydrogen peroxide in water; acetonitrile
T=-20°C; 24 h; Inert atmosphere;
3: With hydrogenchloride in water; acetonitrile
T=0 - 20°C; 0.25 h; Inert atmosphere;
参考文献
Watanabe, Eiichi; Kaiho, Atsushi; Kusama, Hiroyuki; Iwasawa, Nobuharu
Journal of the American Chemical Society, 2013 , vol. 135, # 32 p. 11744 - 11747
